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USGS2011

Performance of ground-penetrating radar on granitic regoliths with different mineral composition

Although ground-penetrating radar (GPR) is extensively used to characterize the regolith, few studies have addressed the effects of chemical and mineralogical compositions of soils and bedrock on its performance. This investigation evaluated the performance of GPR on two different granitic regoliths of somewhat different mineralogical composition in the San Jacinto Mountains of southern California. Radar records collected at a site where soils are Alfisols were more depth restricted than the radar record obtained at a site where soils are Entisols. Although the Alfisols contain an argillic horizon, and the Entisols have no such horizon of clay accumulation, the main impact on GPR effectiveness is related to mineralogy. The bedrock at the Alfisol site, which contains more mafic minerals (5% hornblende and 20% biotite), is more attenuating to GPR than the bedrock at the Entisol site, where mafic mineral content is less (<1% hornblende and 10% biotite). Thus, a relatively minor variation in bedrock mineralogy, specifically the increased biotite content, severely restricts the performance of GPR. Copyright ?? 2011 by Lippincott Williams & Wilkins.

Soil Science↗

USGS2008

NMR and mass spectrometry of phosphorus in wetlands

There is at present little information on the long-term stability of phosphorus sequestered in wetlands. Phosphorus sequestered during high loading periods may be relatively unstable and easily remobilized following changes in nutrient status or hydrological regime, but the chemical forms of sequestered phosphorus that do remobilize are largely unknown at this time. A lack of suitable analytical techniques has contributed to this dearth of knowledge regarding the stability of soil organic phosphorus. We analysed phosphorus in soils from the 'head' of Rescue Strand tree island and an adjacent marsh in the Florida Everglades by 31P nuclear magnetic resonance (NMR) spectroscopy and high-resolution mass spectrometry. Tree islands are important areas of biodiversity within the Everglades and offer a unique opportunity to study phosphorus sequestration because they are exposed to large phosphorus loads and appear to be natural nutrient sinks. The 31P NMR profiling of extracts from surface and sediment samples in the tree island indicates that phosphorus input to Rescue Strand tree island soils is mostly in the form of inorganic ortho-phosphate and is either refractory when deposited or rapidly recycled by the native vegetation into a stable phosphorus pool largely resistant to re-utilization by plants or microbes. Mass spectrometry revealed the presence of inositol hexakisphosphate, a common organic monophosphate ester not previously observed in Everglades' soils. ?? 2008 The Authors.

European Journal of Soil Science↗

USGS2011

Use of airborne hyperspectral imagery to map soil parameters in tilled agricultural fields

Soil hyperspectral reflectance imagery was obtained for six tilled (soil) agricultural fields using an airborne imaging spectrometer (400–2450 nm, ~10 nm resolution, 2.5 m spatial resolution). Surface soil samples ( n = 315) were analyzed for carbon content, particle size distribution, and 15 agronomically important elements (Mehlich-III extraction). When partial least squares (PLS) regression of imagery-derived reflectance spectra was used to predict analyte concentrations, 13 of the 19 analytes were predicted with R 2 > 0.50, including carbon (0.65), aluminum (0.76), iron (0.75), and silt content (0.79). Comparison of 15 spectral math preprocessing treatments showed that a simple first derivative worked well for nearly all analytes. The resulting PLS factors were exported as a vector of coefficients and used to calculate predicted maps of soil properties for each field. Image smoothing with a 3 × 3 low-pass filter prior to spectral data extraction improved prediction accuracy. The resulting raster maps showed variation associated with topographic factors, indicating the effect of soil redistribution and moisture regime on in-field spatial variability. High-resolution maps of soil analyte concentrations can be used to improve precision environmental management of farmlands.

Applied and Environmental Soil Science↗

USGS2018

Thermocouple psychrometry

Thermocouple psychrometry is a technique that infers the water potential of the liquid phase of a sample from measurements within the vapor phase that is in equilibrium with the sample. The theoretical relation between water potential of the liquid phase and relative humidity of the vapor phase is given by the Kelvin equation Ψ = energy/volume = (RT/Vw) ln(p/po) [3.2.3–1] where ψ is water potential (sum of matric and osmotic potential, MPa), R is the universal gas constant (8.314 × 10 -6 MJ mol -1 K -1 ), T is temperature (K), Vw is molar volume of water (1.8 × 10 -5 m 3 mol -1 ), and p/p o is relative humidity expressed as a fraction where p is actual vapor pressure of air in equilibrium with the liquid phase (MPa) and p o is saturation vapor pressure (MPa) at T.

Soil Science Society of America Book Series↗

USGS2018

Miscellaneous methods for measuring matric or water potential

A variety of techniques to measure matric potential or water potential in the laboratory and in the field are described in this section. The techniques described herein require equilibration of some medium whose matric or water potential can be determined from previous calibration or can be measured directly. Under equilibrium conditions the matric or water potential of the medium is equal to that of the soil. The techniques can be divided into: (i) those that measure matric potential and (ii) those that measure water potential (sum of matric and osmotic potentials). Matric potential is determined when the sensor matrix is in direct contact with the soil, so salts are free to diffuse in or out of the sensor matrix, and the equilibrium measurement therefore reflects matric forces acting on the water. Water potential is determined when the sensor is separated from the soil by a vapor gap, so salts are not free to move in or out of the sensor, and the equilibrium measurement reflects the sum of the matric and osmotic forces acting on the water. Seven different techniques are described in this section. Those that measure matric potential include (i) heat dissipation sensors, (ii) electrical resistance sensors, (iii) frequency domain and time domain sensors, and (iv) electro-optical switches. A method that can be used to measure matric potential or water potential is the (v) filter paper method. Techniques that measure water potential include (vi) the Dew Point Potentiameter (Decagon Devices, Inc., Pullman, WA1) (water activity meter) and (vii) vapor equilibration. The first four techniques are electronically based methods for measuring matric potential. Heat dissipation sensors and electrical resistance sensors infer matric potential from previously determined calibration relations between sensor heat dissipation or electrical resistance and matric potential. Frequency-domain and timedomain matric potential sensors measure water content, which is related to matric potential of the sensor through calibration. Electro-optical switches measure changes in light transmission through thin, nylon filters as they absorb or desorb water in response to changes in matric potential. Heat dissipation sensors and electrical resistance sensors are used primarily in the field to provide information on matric potential. Frequency domain matric potential sensors are new and have not been widely used. Time domain matric potential sensors and electro-optical switches are new and have not been commercialized. For the fifth technique, filter paper is used as the standard matrix. The filter paper technique measures matric potential when the filter paper is in direct contact with soil or water potential when separated from soil by a vapor gap. The Dew Point Potentiameter calculates water potential from the measured dew point and sample temperature. The vapor equilibration technique involves equilibration of soil samples with salt solutions of known osmotic potential. The filter paper, Dew Point Potentiameter, and vapor equilibration techniques are generally used in the laboratory to measure water potential of disturbed field samples or to measure water potential for water retention functions.

Soil Science Society of America Book Series↗

USGS1981

Evaluation of Landsat Multispectral Scanner data for mapping vegetated soil landscapes

Landsat multispectral scanner data for Brazos County, Texas, were evaluated in terms of effectiveness for classifying soils on vegetated landscapes at three times during the year: a time of normally adequate soil water, a time of expected soil water deficit, and a time when soil water is normally being replenished. Six test sites were used to evaluate LARSYS supervised and unsupervised classification of vegetated soil landscapes. Open grassland soils were best separated in the fall during a period when soil moisture was being replenished after the summer period of soil water deficit. Woodland soils were separated by Landsat data in late spring when adequate moisture was available. However, a high degree of accuracy was not achieved using Landsat for separating soil map units. Accurate separation of soil mapping units on vegetated landscapes was not possible during late summer when soil water was deficient. Selected soil properties important to plant growth were separable on the test sites using June and October Landsat data. Particle size and soil moisture regime were separated at both dates. Soils with argillic horizons were separated from soils without argillic horizons.

Texas↗

USGS1982

Temperature dependence of unsaturated hydraulic conductivity of two soils

Packed columns of Oakley sand (mixed, mesic Typic Paleudalfs) and Hanford sandy loam (mixed, nonacid, thermic Typic Xerorthents) were used to develop isothermal steady-state fluxes. Soil matric potentials were measured and unsaturated hydraulic conductivities were calculated over a range of matric potentials at 2°, 25°, and 45° ± 0.5°C. In addition, water retention characteristics (to −100 kPa) were measured at these same temperatures for both soils. In this paper, the calculated results are compared to an equation that relates unsaturated conductivity to the intrinsic permeability, the relative permeability, and the viscosity of water. The equation considers viscosity to be the only parameter that changes with temperature. The results show a much greater temperature dependence in the unsaturated conductivity than would be predicted by this equation. The results indicate that the relative permeability may be a function of temperature. The temperature dependence of the soil water matric potential, surface tension, and diffuse double-layer thickness are discussed in terms of their possible interaction with the unsaturated conductivity values obtained. A case is presented for further study to isolate these temperature-sensitive parameters as well as additional parameters related to fluid flow path changes with temperature.

Soil Science Society of America Journal↗

USGS1982

Perched water tables on hillsides in western Oregon: I. Some factors affecting their development and longevity

Perched water tables on hillsides located on the western border of the Willamette Valley in Oregon in some cases have the potential to transport pollutants from either domestic or agricultural sources downslope to streams, ponds, or reservoirs, resulting in the deterioration of the quality of these waters. In this paper, some factors responsible for the development and longevity of these potentially problem-causing perched water tables on three hillsides were examined. Analyses of hydraulic conductivity data and the relationships between rainfall, soil water pressure potential, and time suggest that permeable rock below 110 cm rather than clayey B horizons is mainly responsible for the development of perched water tables on upper convex slope positions on two of these hillsides. The data also suggest that subsurface flow from the upper convex regions contributed significant amounts of water to the lower convex slope positions. Further, perched water tables developed more rapidly, to a greater extent, and lasted longer in upper horizons of a lower concave region of slope where a shallow perched water table was already present at the onset of rainfall. Finally, perched water tables did not develop in the upper horizons on a third hillside that had no impermeable regions in the soil or upper rock mantle.

Oregon↗

USGS1982

Perched water tables on hillsides in western Oregon: II. Preferential downslope movement of water and anions

Perched water tables on hillsides in western Oregon potentially provide a means by which pollutants from agricultural and domestic sources may enter surface waters and consequently degrade the quality of these waters. This paper reports the results of experiments which were carried out to investigate the flow of solutes and water from buried line sources in and above perched water tables on three different hillsides in western Oregon. In the saturated soil and rock mantles of two hillsides, evidence suggests that water and solutes flow preferentially through large continuous voids. The evidence includes the very high maximum rate of anion movement downslope, the failure of pore velocities calculated from Darcy's Law to predict the rate and direction of anion movement, the short time before high levels of anions are detected downslope, and the spatial variability in the maximum rates of anion movement over the depth and width of sites. On the third hillside, tracer anion movement and soil water pressure measurements indicate that preferential flow occurs through large continuous pores during heavy rainfall while the surrounding soil and rock mantle remains unsaturated. Finally, experiments with Rodamine WT dye show that a variety of continuous voids of different origins and sizes conduct water and solutes preferentially in the soil and upper regions of rock on these hillsides.

Oregon↗

USGS1984

Submersible pressure outflow cell for measurement of soil water retention and diffusivity from 5 to 95 degrees C

A technique was developed to measure water content in soil as a function of capillary pressure from 5 to 95°C. To overcome problems encountered at high temperature, a modified Tempe pressure cell containing a soil sample is suspended in a constant-temperature water bath. The cell's porous plate is in direct contact with circulating bath water, thus eliminating the problem of entrapped air bubbles. A balance located above the water bath measures water content changes in the soil by weighing the entire pressure cell under water. The technique is designed to measure soil water retention characteristics and to make transient outflow estimates of the soil water diffusivity at temperatures from 5 to 95°C. We also used the technique to determine the isobaric temperature dependence of water retention in soil. Results indicate that at constant capillary pressure, the relationship between moisture content and temperature is hysteretic.

Soil Science Society of America Journal↗

USGS1985

The occurrence of extractable elements in soils from the northern Great Plains

The modes of occurrence of extractable elements from 21 A and C horizon samples of uncultivated soils were examined using R-mode factor analysis. The extractants (DTPA, EDTA, HCl, hydroquinone, magnesium nitrate, and ammonium oxalate) cover a wide range of chemical attack. Four major elements (Ca, K, Mg, and Na) and eight trace elements (Cd, Co, Cu, Fe, Mn, Ni, Pb, and Zn) were determined in each extractant solution. A variety of chemical, mineralogical, and physical variables were also determined on each sample. Four varimax factors (clay, organic, Fe and Mn oxides, and soluble-Na) accounted for 74.2% of the total variance of the 90 variables for the A horizon. Seven varimax factors (Fe and Mn oxides, clay, CEC, soluble-Na, organic, Fe and Mn, and plagioclase) accounted for 77.2% of the total variance of the 79 variables for the C horizon. A and C horizon extractable trace elements are most generally related to Fe and Mn oxides, as indicated by loadings on the Fe and Mn oxide factor for both the A and C horizons. Each extractant generally operates on different modes of occurrence of an element in soil. For example, substantial differences occur between the HCl-, oxalate-, and hydroquinone-extractable trace elements. However, the modes of occurrence for trace elements removed by DTPA and EDTA were very similar, suggesting strong relationships between elements dissolved by these two extractants. The modes of occurrence for each individual major element are similar with each of the six extractants. A horizon Ca and Mg, and C horizon K and Mg are strongly related to a clay factor. C horizon Ca and A horizon K are strongly related to the CEC and organic factors, respectively. Both A and C horizon extractable Na are very strongly related to the soluble-Na factor. These results suggest that extractable major elements are water-soluble and are associated with the constituents that are responsible for that factor. Consequently, strong relationships should occur for any individual major element dissolved by any pair of extractants.

northern Great Plains↗

USGS1985

Use of Peltier coolers as soil heat flux transducers

Peltier coolers were modified and calibrated to serve as soil heat flux transducers. The modification was to fill their interiors with epoxy. The average calibration constant on 21 units was 13.6 ± 0.8 kW m −2 V −1 at 20°C. This sensitivity is about eight times that of the two thermopile transducers with which comparisons were made. The temperature coefficients of the Peltier cooler transducers avg −0.034 kW m −2 V −1 °C −1 , whereas those of the two thermopile transducers were only 25% as large, relative to their calibration constants. The thermal conductivity of the Peltier cooler transducers was 0.4 W m −1 °C −1 , which is comparable to that of dry soil. The cost of an unmodified Peltier cooler is around 20 dollars.

Soil Science Society of America Journal↗

USGS1985

Geophysical techniques for reconnaissance investigations of soils and surficial deposits in mountainous terrain

Two techniques were assessed for their capabilities in reconnaissance studies of soil characteristics: depth to the water table and depth to bedrock beneath surficial deposits in mountainous terrain. Ground-penetrating radar had the best near-surface resolution in the upper 2 m of the profile and provided continuous interpretable imagery of soil profiles and bedrock surfaces. Where thick colluvium blankets side slopes, the GPR could not consistently define the bedrock interface. In areas with clayey or shaley sediments, the GPR is also more limited in defining depth and is less reliable. Seismic refraction proved useful in determining the elevation of the water table and depth to bedrock, regardless of thickness of overlying material, but could not distinguish soil-profile characteristics.

Soil Science Society of America Journal↗

USGS1986

The temperature dependence of isothermal moisture vs. potential characteristics of soils

A method has been developed for rapid, transient measurement of hysteretic soil-moisture characteristics as a function of temperature. While a varying soil-water pressure was imposed on a thin sample by means of flexible membranes held in firm contact with the soil, water content was measured by gamma-ray attenuation, and matric potential was measured with tensiometers. The applied pressure was cycled through a program designed to obtain hysteretic θ(ψ) main and scanning curves. Isothermal characteristics were measured for 181-µm glass beads, Plainfield (Typic Udipsamments) sand, and an undisturbed core of Plano (Typic Argiudolls) silt loam at several temperatures in the 4° to 50°C range. At each temperature the measurements included main drying and wetting curves covering the θ range from 0.30 to 0.05 m 3 water/m 3 for glass beads, 0.30 to 0.17 for sand, and 0.45 to 0.37 for silt loam. A model has been developed to quantify the temperature dependence as a function of θ. Combined with an isothermal hysteresis model of Mualem, this model requires only three characteristic functions to represent all hysteretic θ(ψ) curves for a given medium at all temperatures. Model calculations for the sand and silt loam data indicate that except near saturation, the temperature effect is greater than can be accounted for by the temperature dependence of the surface tension of pure water. The results rule out several possible explanations but they support the hypothesis that the concentration and effectiveness of dissolved surfactants increases with temperature.

Soil Science Society of America Journal↗

USGS1986

Transport of chloride ion in a water-unsaturated soil exhibiting anion exclusion

Miscible displacement techniques were used to create Cl - concentration profiles in unsaturated laboratory columns of Delhi sand (Typic Xeropsamments), each having a nearly uniform water content. The three steady flow rates used resulted in three different, average water contents. Chloride concentrations near the top of the column were smaller and penetration of Cl - in the column was deeper than expected assuming that Cl - is a noninteracting solute. Such observations indicate the presence of anion exclusion. This interpretation is further substantiated by chloride and tritium breakthrough curves obtained from a saturated column of the same soil. The saturated experiments show that tritium occupies the entire measured pore volume of the column, but that Cl - is restricted to a smaller pore volume. The formulation of the conventional convection-dispersion theory for solute transport in soil which includes anion exclusion resulted in model calculations that fitted the unsaturated Cl - concentration profiles quite well. The dispersion coefficients obtained for the unsaturated profiles increase with water velocity and are lower than those previously reported for comparable water velocities in the same but saturated soil. The dispersivity of the unsaturated soil is also smaller than that reported for the saturated soil. For the experimental conditions used, the effective Cl - exclusion volume was found to be independent of water content and velocity and occupied about ten percent of the unsaturated water content.

Soil Science Society of America Journal↗

USGS1986

Recovery of compacted soils in Mojave Desert ghost towns

Residual compaction of soils was measured at seven sites in five Mojave Desert ghost towns. Soils in these Death Valley National Monument townsites were compacted by vehicles, animals, and human trampling, and the townsites had been completely abandoned and the buildings removed for 64 to 75 yr. The soils studied (generally sandy, mixed, Typic Calciorthids) were derived from granitic or volcanic alluvium at elevations from 1310 to 1730 m. Compaction measurements in the townsites, including penetration depth, penetration resistance, bulk density, and peak shear stress, indicated that only one site had completely recovered to ambient soil conditions after 75 yr. Recovery times extrapolated using a linear recovery model ranged from 80 to 140 yr and averaged 100 yr. The recovery times were related to elevation, suggesting freeze-thaw loosening as an important factor in ameliorating soil compaction in the Mojave Desert.

California↗

USGS1987

An automated technique for flow measurements from mariotte reservoirs

The mariotte reservoir supplies water at a constant hydraulic pressure by self-regulation of its internal gas pressure. Automated outflow measurements from mariotte reservoirs are generally difficult because of the reservoir's self-regulation mechanism. This paper describes an automated flow meter specifically designed for use with mariotte reservoirs. The flow meter monitors changes in the mariotte reservoir's gas pressure during outflow to determine changes in the reservoir's water level. The flow measurement is performed by attaching a pressure transducer to the top of a mariotte reservoir and monitoring gas pressure changes during outflow with a programmable data logger. Using a simple linear relation between reservoir gas pressure and water-level changes with time, the data logger converts the transducer signal into outflow-flux values. To demonstrate the usefulness of the new technique, two constant-head experiments are described that have vastly different flux ranges and time durations. The first experiment was a 1-h infiltration run in which infiltration rates dropped from 0.6 to 0.2 cm/min. The second experiment was a 3-week evaporation experiment in which the evaporation rate ranged from 1.0 to 3.0 cm/d. Results indicate that the automated flow measurement technique performed well when compared to a manual sight-tube technique for flux measurements; the difference between the two methods was never more than 9% for the infiltration experiment and 5% for the evaporation experiment. The advantages of the new technique over previously available automated flow measurement techniques include: (i) the ability to rapidly record a large range of fluxes without restricting outflow, and (ii) the ability to accurately average the pulsing flow, which commonly occurs during outflow from the mariotte reservoir.

Soil Science Society of America Journal↗

USGS1987

Determination of Fe(III) and Fe(II) in oxalate extracts of sediment

A method was developed to determine the concentrations of oxalate-extractable Fe(III) and Fe(II) in sediments. Sediment was extracted in acid ammonium oxalate under N 2 . Iron(II) in the extract was determined with ferrozine. Iron(III) in the extract was reduced with hydroxylamine-hydrochloride, and total Fe in the extract was determined with ferrozine. Oxalate-extractable Fe(III) was calculated as the difference between Fe(II) and total Fe in the extract. Iron(II) was not oxidized, and Fe(III) was not reduced during the extraction. For an accurate estimate of oxalate-extractable Fe(III), fresh samples had to be analyzed, because air-drying or freeze-drying the samples oxidized Fe(II) to oxalate-extractable Fe(III). With a minimal increase in analytical effort, the method yields far more information on Fe geochemistry than the standard aerobic oxalate extraction method.

Soil Science Society of America Journal↗