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At least 91 records · Page 5Linked to original sources
USGS2001

Methods of analysis by the U. S. Geological Survey National Water Quality Laboratory-Determination of organic plus inorganic mercury in filtered and unfiltered natural water with cold vapor; atomic fluorescence spectrometry

An analytical method using cold vapor-atomic fluorescence spectrometry was developed by the U.S. Geological Survey in 2001 for the determination of organic plus inorganic mercury in filtered and unfiltered natural water. This method was developed to eliminate the use of acid dichromate preservative and to provide capability to measure ambient mercury concentrations in natural water. Dissolved mercury includes all oxidizable mercury species present in natural water that has been filtered through a 0.45- micrometer pore size capsule filter. Wholewater recoverable mercury includes dissolved mercury species and mercury species adsorbed to particulate matter in unfiltered natural water. Mercury species can include elemental mercury, mercury (II), mercury (II) complexes, various alkyl- and phenylmercury compounds, and other forms of mercury. In this method, samples are collected and processed according to standard U.S. Geological Survey protocols. Samples are preserved onsite with 6N hydrochloric acid in a ratio of 1 to 100 in a borosilicateglass bottle with fluoropolymer-lined cap. Mercury species are oxidized to mercury (II) by using bromine monochloride; excess oxidation reagent is neutralized with hydroxylamine hydrochloride. Elemental mercury produced after adding stannous chloride is purged from the solution with ultrapure argon gas into a cell in which the mercury concentration is measured by atomic fluorescence emission at 253.7 nanometers. The analytical response is linear up to 125 nanograms per liter (ng/L) of mercury, and the short-term method detection limit is about 5 ng/L. The analytical variability at 50 ng/L is about 10 percent. This report describes the method and compares the use of hydrochloric acid to acid dichromate as a field preservative. Ambient mercury concentrations in hydrochloric acidpreserved samples stored in borosilicate-glass bottles with fluoropolymer-lined caps are shown to be stable for at least 30 days. Mercury concentrations are stable for at least 5 months after bromine monochloride is added to the sample bottles in the laboratory. The long-term average percent recoveries at 20, 45, and 75 ng/L in reagent water, filtered and unfiltered ground water, and filtered and unfiltered surface water range from 89 to 108, 96 to 103, and 94 to 98 percent, respectively.

Water-Resources Investigations Report↗
USGS2008

Biodegradation in contaminated aquifers: Incorporating microbial/molecular methods

In order to evaluate natural attenuation in contaminated aquifers, there has been a recent recognition that a multidisciplinary approach, incorporating microbial and molecular methods, is required. Observed decreases in contaminant mass and identified footprints of biogeochemical reactions are often used as evidence of intrinsic bioremediation, but characterizing the structure and function of the microbial populations at contaminated sites is needed. In this paper, we review the experimental approaches and microbial methods that are available as tools to evaluate the controls on microbially mediated degradation processes in contaminated aquifers. We discuss the emerging technologies used in biogeochemical studies and present a synthesis of recent studies that serve as models of integrating microbiological approaches with more traditional geochemical and hydrogeologic approaches in order to address important biogeochemical questions about contaminant fate.

Groundwater↗
USGS1989

Reconnaissance estimates of natural recharge to desert basins in Nevada, U.S.A., by using chloride-balance calculations

A chloride-balance method for estimating average natural recharge to groundwater basins in the Basin and Range Province of the western United States may be a useful alternative or complement to current techniques. The chloride-balance method, as presented in this paper, equates chloride in recharge water and runoff to chloride deposited in mountainous recharge-source areas by precipitation and dry fallout. Given estimates of annual precipitation on these source areas and chloride concentrations of bulk precipitation and recharge water, the rate of recharge can be estimated providing that: (1) no other major sources of chloride exist; (2) direct runoff to discharge areas in the basin is small or can otherwise be taken in account in the balance; and (3) the recharge sources for the basin are correctly delineated. The estimates are sensitive to the estimated rate of input of chloride from the atmosphere; this is the greatest data need for future applications of the method. Preliminary applications of the method to sixteen basins in Nevada, including Las Vegas Valley, indicate that the method can be a useful tool for hydrologists and resource managers. Correlation coefficients between recharge efficiencies for the basins - estimated on the basis of recharge estimates that use the chloride-balance method and two other currently used techniques - range from 0.54 to 0.95, depending on assumptions about where the method may be applied.

Nevada↗
USGS2013

Candidate soil indicators for monitoring the progress of constructed wetlands toward a natural state: a statistical approach

A persistent question among ecologists and environmental managers is whether constructed wetlands are structurally or functionally equivalent to naturally occurring wetlands. We examined 19 variables collected from 10 constructed and nine natural emergent wetlands in Ohio, USA. Our primary objective was to identify candidate indicators of wetland class (natural or constructed), based on measurements of soil properties and an index of vegetation integrity, that can be used to track the progress of constructed wetlands toward a natural state. The method of nearest shrunken centroids was used to find a subset of variables that would serve as the best classifiers of wetland class, and error rate was calculated using a five-fold cross-validation procedure. The shrunken differences of percent total organic carbon (% TOC) and percent dry weight of the soil exhibited the greatest distances from the overall centroid. Classification based on these two variables yielded a misclassification rate of 11% based on cross-validation. Our results indicate that % TOC and percent dry weight can be used as candidate indicators of the status of emergent, constructed wetlands in Ohio and for assessing the performance of mitigation. The method of nearest shrunken centroids has excellent potential for further applications in ecology.

Ohio↗
USGS2015

Prospective HyspIRI global observations of tidal wetlands

Tidal wetlands are highly productive and act as critical habitat for a wide variety of plants, fish, shellfish, and other wildlife. These ecotones between aquatic and terrestrial environments also provide protection from storm damage, run-off filtering, and recharge of aquifers. Many wetlands along coasts have been exposed to stress-inducing alterations globally, including dredge and fill operations, hydrologic modifications, pollutants, impoundments, fragmentation by roads/ditches, and sea level rise. For wetland protection and sensible coastal development, there is a need to monitor these ecosystems at global and regional scales. Recent advances in satellite sensor design and data analysis are providing practical methods for monitoring natural and man-made changes in wetlands. However, available satellite remote sensors have been limited to mapping primarily wetland location and extent. This paper describes how the HyspIRI hyperspectral and thermal infrared sensors can be used to study and map key ecological properties, such as species composition, biomass, hydrology, and evapotranspiration of tidal salt and brackish marshes and mangroves, and perhaps other major wetland types, including freshwater marshes and wooded/shrub wetlands.

Remote Sensing of Environment↗
USGS2022

Human-in-the-Loop segmentation of earth surface imagery

Segmentation, or the classification of pixels (grid cells) in imagery, is ubiquitously applied in the natural sciences. Manual methods are often prohibitively time-consuming, especially those images consisting of small objects and/or significant spatial heterogeneity of colors or textures. Labeling complicated regions of transition that in Earth surface imagery are represented by collections of mixed-pixels, -textures, and -spectral signatures, can be especially error-prone because it is difficult to reliably unmix, identify and delineate consistently. However, the success of supervised machine learning (ML) approaches is entirely dependent on good label data. We describe a fast, semi-automated, method for interactive segmentation of N-dimensional (x, y, N) images into two-dimensional (x, y) label images. It uses human-in-the-loop ML to achieve consensus between the labeler and a model in an iterative workflow. The technique is reproducible; the sequence of decisions made by human labeler and ML algorithms can be encoded to file, so the entire process can be played back and new outputs generated with alternative decisions and/or algorithms. We illustrate the scientific potential of segmentation of imagery of diverse settings and image types using six case studies from river, estuarine, and open coast environments. These photographic and non-photographic imagery consist of 1- and 3-bands on regular and irregular grids ranging from centimeters to tens of meters. We demonstrate high levels of agreement in label images generated by several labelers on the same imagery, and make suggestions to achieve consensus and measure uncertainty, ideal for widespread application in training supervised ML for image segmentation.

Earth and Space Science↗
USGS2021

Health surveillance of a potential bridge host: Pathogen exposure risks posed to avian populations augmented with captive-bred pheasants

Augmentation of wild populations with captive-bred individuals presents an inherent risk of co-introducing novel pathogens to naïve species, but it can be an important tool for supplementing small or declining populations. Game species used for human enterprise and recreation such as the ring-necked pheasant ( Phasianus colchicus ) are commonly raised in captivity and released onto public and private wildlands as a method of augmenting naturalized pheasant populations. This study presents findings on pathogen exposure from three sources of serological data collected in California during 2014–2017 including (a) 71 pen-reared pheasants sampled across seven game bird breeding farms, (b) six previously released pen-reared pheasants captured at two study sites where wild pheasants occurred and (c) 79 wild pheasants captured across six study sites. In both pen-reared and wild pheasants, antibodies were detected against haemorrhagic enteritis virus (HEV), infectious laryngotracheitis (ILT), infectious bursal disease virus (IBDV), paramyxovirus type 1 (PMV-1) and Pasteurella multocida (PM). Previously released pen-reared pheasants were seropositive for HEV, ILT, and PM. Generalized linear mixed models accounting for intraclass correlation within groups indicated that pen-reared pheasants were more than twice as likely to test positive for HEV antibodies. Necropsy and ancillary diagnostics were performed in addition to serological testing on 40 pen-reared pheasants sampled from five of the seven farms. Pheasants from three of these farms tested positive by PCR for Siadenovirus, the causative agent of both haemorrhagic enteritis in turkeys and marble spleen disease of pheasants, which are serologically indistinguishable. Following necropsy, owners from the five farms were surveyed regarding husbandry and biosecurity practices. Farms ranged in size from 10,000 to more than 100,000 birds, two farms raised other game bird species on premises, and two farms used some form of vaccination. Biosecurity practices varied by farm, but the largest farm implemented the strictest practices.

California↗
USGS1985

Regional magnetotelluric surveys in hydrocarbon exploration, Parana Basin, Brazil

The magnetotelluric geophysical method has been used effectively as a hydrocarbon exploration tool in the intracratonic Parana basin of South America. The Parana basin has an area of about 1,200,000 km 2 (463,000 mi 2 ), extending over portions of Brazil, Paraguay, Uruguay, Argentina, and Bolivia. The Paleozoic marine sedimentary rocks in the Parana basin are covered by the world's most extensive flood basalt complex, making geophysical exploration extremely difficult, although modern seismic techniques recently applied are achieving good results in some areas. The 1-2 km (3,300-6,600 ft) thick surface basalts and buried diabase sills pose no problem for the magnetotelluric method because the natural electromagnetic fields used as the energy source pass easily through the basalt. Data for the regional study were taken on six profiles with soundings spaced 8 to 15 km (5 to 9 mi) apart. The magnetotelluric sounding data outline a linear uplift known as the Ponta Grossa arch. This major structural feature cuts across the northeast-trending intracratonic basin almost perpendicularly, and is injected with numerous diabase dikes. Although its character is reasonably well known in the shallow, eastern parts of the basin, it is poorly delineated in the deeper parts of the basin where promising natural gas zones have been tested in several wells. In the survey area, MT interpretations show that basalts have aggregate thickness of as much as 2 km (6,600 ft), and basement may be as much as 6 km (20,000 ft) below the surface. Over most of the basin, the basalts are covered by Upper Cretaceous to Holocene continental sediments of a few hundred meters thickness and are underlain by 2 to 4 km (6,600 to 13,100 ft) thick Paleozoic sediments with possible hydrocarbon potential. The Ponta Grossa arch is interpreted to be the failed arm of a triple rift system that formed during the separation of the African and South American continents. Shales of the Devonian Ponta Grossa Formation are important Parana basin source rocks for hydrocarbons, as are several Permian units. Significant electrical contrasts occur between the Permian sediments and older units, so that magnetotelluric measurements can give an indication of the regional thickness of the Permian and younger sediments to aid in interpreting hydrocarbon migration patterns and possible trap areas.

Parana Basin↗
USGS2006

Use of Numerical Simulations in Surface-Water Studies by the U.S. Geological Survey in Missouri

Numerical simulations of surface-water systems can be a useful tool to predict and understand a variety of physical, chemical, and ecological processes. A number of applications have been conducted by the U.S. Geological Survey Missouri Water Science Center in conjunction with ecological and flood studies in Missouri. Numerical simulations can provide a physically based method to predict natural processes in situations where it is impractical to measure the results directly as a result of cost, time, or infrequent occurrence. Numerical simulations provide a means of analyzing 'What if?' scenarios. For example, a simulation can be used to estimate the effects of reservoirs in a basin on the timing and magnitude of downstream streamflows. Simulations also may provide a better understanding of a complex process, such as sediment transport and deposition during a large flood. Alternatively, numerical simulations can be used to quantify aquatic habitat that is defined by the hydraulic (depth and velocity) characteristics of streamflow. This report provides information on recent applications of numerical simulations of hydraulic, floodplain, and watershed processes.

Fact Sheet↗
USGS2010

USGS Toxic Substances Hydrology Program, 2010

The U.S. Geological Survey (USGS) Toxic Substances Hydrology Program adapts research priorities to address the most important contamination issues facing the Nation and to identify new threats to environmental health. The Program investigates two major types of contamination problems: * Subsurface Point-Source Contamination, and * Watershed and Regional Contamination. Research objectives include developing remediation methods that use natural processes, characterizing and remediating contaminant plumes in fractured-rock aquifers, identifying new environmental contaminants, characterizing new and understudied pesticides in common pesticide-use settings, explaining mercury methylation and bioaccumulation, and developing approaches for remediating watersheds affected by active and historic mining.

Fact Sheet↗
USGS1971

Map showing locations of samples dated by radiocarbon methods in the San Francisco Bay region

Radiocarbon dating is an important interdisciplinary tool for studies involving events and processes during the last 40,000 years of earth history, including studies involving marine transgressions and regressions, land subsidence, climatic changes, sedimentation rates and patterns, fault movements, and archaeology, among others. The potential value of a radiocarbon date is diminished, however, if adequate site data are not taken with the sample and do not accompany the date in publication. At a minimum, published dates should include an accurate location for the dated sample, type of material dated and method of dating, nature of the site, depth below surface (or other accurately defined datum) of date sample, stratigraphy of material overlying date sample, and the significance of the data in the study.

California↗
USGS2025

Methodology and technical input for the 2025 U.S. List of Critical Minerals—Assessing the potential effects of mineral commodity supply chain disruptions on the U.S. economy

The Secretary of the Interior, acting through the Director of the U.S. Geological Survey, is tasked by section 7002 (“Mineral Security”) of title VII (“Critical Minerals”) of the Energy Act of 2020 (Public Law 116–260, December 27, 2020, 116th Congress) with reviewing and revising the methodology used to evaluate mineral commodity supply risk and the U.S. List of Critical Minerals (LCM) no less than every 3 years. Following two previous LCM assessments, this analysis represents the latest technical input for evaluating each mineral commodity’s supply risk and determining their recommended status on the LCM. We evaluated mineral commodity supply risk using two criteria: (1) an economic effects assessment that quantified the potential effects of various trade disruption scenarios on the U.S. economy, and (2) an examination of whether the mineral commodity’s U.S. supply chain relied on a sole domestic producer that represented a single point of failure. For the first criterion, postdisruption equilibrium quantities and prices for each mineral commodity were calculated based on their price elasticities of supply and demand and the availability of excess production capacity for each yearlong foreign trade disruption scenario. Subsequently, a nonlinear optimization routine was used with detailed economic input-output tables to estimate the potential economic effects on the U.S. economy of over 1,200 scenarios for 84 mineral commodities. After accounting for the probability of each scenario’s occurrence, the overall results are presented in terms of changes in U.S. gross domestic product (GDP) by individual industry and the economy overall. The results, which ranged from a net decrease in U.S. GDP of nearly $4.5 billion to a net increase of $33 million, largely reflect U.S. import dependency and world production concentration. Using the Jenks natural breaks optimization method, a statistical classification technique, we categorized the mineral commodities into several classes based on this overall risk quantification. Mineral commodities with annualized probability-weighted net decreases in U.S. GDP greater than $2 million were recommended for inclusion on the LCM. If a mineral commodity did not meet the threshold for inclusion on the LCM under the first criterion, its domestic supply chain was examined under the second criterion, which recommended a mineral commodity for inclusion on the LCM if there was only a single domestic producer. Ultimately, the two criteria resulted in the recommendation of the addition of six mineral commodities (in descending risk order, potash, silicon, copper, silver, rhenium, and lead) to and the removal of two mineral commodities (arsenic and tellurium) from the LCM. By using an economic effects assessment, the results of this analysis provide a prioritization that can also be compared directly against other risk analyses and the cost of various risk mitigation strategies.

Open-File Report↗
USGS2000

Methods of analysis by the U.S. Geological Survey National Water Quality Laboratory-Determination of whole-water recoverable arsenic, boron, and vanadium using inductively coupled plasma-mass spectrometry

Analysis of in-bottle digestate by using the inductively coupled plasma?mass spectrometric (ICP?MS) method has been expanded to include arsenic, boron, and vanadium. Whole-water samples are digested by using either the hydrochloric acid in-bottle digestion procedure or the nitric acid in-bottle digestion procedure. When the hydrochloric acid in-bottle digestion procedure is used, chloride must be removed from the digestate by subboiling evaporation before arsenic and vanadium can be accurately determined. Method detection limits for these elements are now 10 to 100 times lower than U.S. Geological Survey (USGS) methods using hydride generation? atomic absorption spectrophotometry (HG? AAS) and inductively coupled plasma? atomic emission spectrometry (ICP?AES), thus providing lower variability at ambient concentrations. The bias and variability of the methods were determined by using results from spike recoveries, standard reference materials, and validation samples. Spike recoveries in reagent-water, surface-water, ground-water, and whole-water recoverable matrices averaged 90 percent for seven replicates; spike recoveries were biased from 25 to 35 percent low for the ground-water matrix because of the abnormally high iron concentration. Results for reference material were within one standard deviation of the most probable value. There was no significant difference between the results from ICP?MS and HG?AAS or ICP?AES methods for the natural whole-water samples that were analyzed.

Open-File Report↗
USGS2007

Environmental Setting of the Granger Drain and DR2 Basins, Washington, 2003-04

The Granger Drain and DR2 basins are located in the Yakima River basin in south central Washington. These agricultural basins are one of five areas in the United States selected for study as part of the National Water-Quality Assessment Program Agricultural Chemicals: Source, Transport, and Fate Study. The Program is designed to describe water-quality conditions and trends based on representative surface- and ground-water resources across the Nation. The objective of the Agricultural Chemicals topical study is to investigate the sources, transport, and fate of selected agricultural chemicals in a variety of agriculturally diverse environmental settings. The Granger Drain and DR2 basins were selected for the Agricultural Chemicals topical study because they represent the irrigated agricultural setting that characterizes eastern Washington. These basins are located in one of the most productive agricultural areas in the United States. This report describes the environmental setting of the Granger Drain and DR2 basins in the context of how agricultural practices, including agricultural chemical applications and irrigation methods, interface with natural settings and hydrologic processes.

Scientific Investigations Report↗
USGS2002

Experimental Acoustic Velocity Measurements in a Tidally Affected Stream

The U.S. Geological Survey (USGS) constructed a continuous steamgaging station on the tidally affected Escatawpa River at Interstate 10 near Orange Grove, Mississippi, in August 2001. The gage collects water quantity parameters of stage and stream velocity, and water quality parameters of water temperature, specific conductance, and salinity. Data are transmitted to the local USGS office via the GOES satellite and are presented on a near real-time web page. Due to tidal effects, the stream has multiple flow regimes which include downstream, bi-directional, and reverse flows. Advances in acoustic technology have made it possible to gage streams of this nature where conventional methods have been unsuccessful. An experimental mount was designed in an attempt to recognize, describe, and quantify these flow regimes by using acoustic Doppler equipment.

Conference Paper↗
USGS2015

From mobile ADCP to high-resolution SSC: a cross-section calibration tool

Sediment is a major cause of stream impairment, and improved sediment monitoring is a crucial need. Point samples of suspended-sediment concentration (SSC) are often not enough to provide an understanding to answer critical questions in a changing environment. As technology has improved, there now exists the opportunity to obtain discrete measurements of SSC and flux while providing a spatial scale unmatched by any other device. Acoustic instruments are ubiquitous in the U.S. Geological Survey (USGS) for making streamflow measurements but when calibrated with physical sediment samples, they may be used for sediment measurements as well. The acoustic backscatter measured by an acoustic Doppler current profiler (ADCP) has long been known to correlate well with suspended sediment, but until recently, it has mainly been qualitative in nature. This new method using acoustic surrogates has great potential to leverage the routine data collection to provide calibrated, quantitative measures of SSC which hold promise to be more accurate, complete, and cost efficient than other methods. This extended abstract presents a method for the measurement of high spatial and temporal resolution SSC using a down-looking, mobile ADCP from discrete cross-sections. The high-resolution scales of sediment data are a primary advantage and a vast improvement over other discrete methods for measuring SSC. Although acoustic surrogate technology using continuous, fixed-deployment ADCPs (side-looking) is proven, the same methods cannot be used with down-looking ADCPs due to the fact that the SSC and particle-size distribution variation in the vertical profile violates theory and complicates assumptions. A software tool was developed to assist in using acoustic backscatter from a down-looking, mobile ADCP as a surrogate for SSC. This tool has a simple graphical user interface that loads the data, assists in the calibration procedure, and provides data visualization and output options. This tool is designed to improve ongoing efforts to monitor and predict resource responses to a changing environment. Because ADCPs are used routinely for streamflow measurements, using acoustic backscatter from ADCPs as a surrogate for SSC has the potential to revolutionize sediment measurements by providing rapid measurements of sediment flux and distribution at spatial and temporal scales that are far beyond the capabilities of traditional physical samplers.

Conference Paper↗
USGS2002

Corn leaf nitrate reductase - A nontoxic alternative to cadmium for photometric nitrate determinations in water samples by air-segmented continuous-flow analysis

Development, characterization, and operational details of an enzymatic, air-segmented continuous-flow analytical method for colorimetric determination of nitrate + nitrite in natural-water samples is described. This method is similar to U.S. Environmental Protection Agency method 353.2 and U.S. Geological Survey method 1-2545-90 except that nitrate is reduced to nitrite by soluble nitrate reductase (NaR, EC 1.6.6.1) purified from corn leaves rather than a packed-bed cadmium reactor. A three-channel, air-segmented continuous-flow analyzer-configured for simultaneous determination of nitrite (0.020-1.000 mg-N/L) and nitrate + nitrite (0.05-5.00 mg-N/L) by the nitrate reductase and cadmium reduction methods-was used to characterize analytical performance of the enzymatic reduction method. At a sampling rate of 90 h-1, sample interaction was less than 1% for all three methods. Method detection limits were 0.001 mg of NO2- -N/L for nitrite, 0.003 mg of NO3-+ NO2- -N/L for nitrate + nitrite by the cadmium-reduction method, and 0.006 mg of NO3- + NO2- -N/L for nitrate + nitrite by the enzymatic-reduction method. Reduction of nitrate to nitrite by both methods was greater than 95% complete over the entire calibration range. The difference between the means of nitrate + nitrite concentrations in 124 natural-water samples determined simultaneously by the two methods was not significantly different from zero at the p = 0.05 level.

Environmental Science & Technology↗
USGS2024

Penguin colony georegistration using camera pose estimation and phototourism

Satellite-based remote sensing and uncrewed aerial imagery play increasingly important roles in the mapping of wildlife populations and wildlife habitat, but the availability of imagery has been limited in remote areas. At the same time, ecotourism is a rapidly growing industry and can yield a vast catalog of photographs that could be harnessed for monitoring purposes, but the inherently ad-hoc and unstructured nature of these images make them difficult to use. To help address this, a subfield of computer vision known as phototourism has been developed to leverage a diverse collection of unstructured photographs to reconstruct a georeferenced three-dimensional scene capturing the environment at that location. Here we demonstrate the use of phototourism in an application involving Antarctic penguins, sentinel species whose dynamics are closely tracked as a measure of ecosystem functioning, and introduce a semi-automated pipeline for aligning and registering ground photographs using a digital elevation model (DEM) and satellite imagery. We employ the Segment Anything Model (SAM) for the interactive identification and segmentation of penguin colonies in these photographs. By creating a textured 3D mesh from the DEM and satellite imagery, we estimate camera poses to align ground photographs with the mesh and register the segmented penguin colony area to the mesh, achieving a detailed representation of the colony. Our approach has demonstrated promising performance, though challenges persist due to variations in image quality and the dynamic nature of natural landscapes. Nevertheless, our method offers a straightforward and effective tool for the georegistration of ad-hoc photographs in natural landscapes, with additional applications such as monitoring glacial retreat.

PLoS ONE↗