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USGS2020

Estimating wildfire fuel consumption with multitemporal airborne laser scanning data and demonstrating linkage with MODIS-derived fire radiative energy

Characterizing pre- and post-fire fuels remains a key challenge for estimating biomass consumption and carbon emissions from wildfires. Airborne laser scanning (ALS) data have demonstrated effectiveness for estimating canopy, and to a lesser degree, surface fuel components at fine-scale (i.e., 30 m) across landscapes. Using pre- and post-fire ALS data and corresponding field data, this study estimated consumption of canopy fuel (ΔCF), understory fuel (ΔUF), total fuel (ΔTF), and canopy bulk density (ΔCBD) for the 2012 Pole Creek fire in Oregon, USA (10,760 ha), and portions of the 2011 Las Conchas fire in New Mexico, USA (4,934 ha). Additionally, the feasibility of predicting fuel consumption was tested using separate pre- and post-fire models (PrePost), models combining all pre- and post-fire data (Pooled), and models using all data from both fires (Global). Estimates of ΔTF were then compared to fire radiative energy (FRE, units: MJ) derived from Fire Radiative Power (FRP, units: MW) observations from the Moderate Resolution Imaging Spectroradiometer (MODIS) sensor onboard NASA Terra and Aqua satellites to mechanistically derive a biomass combustion coefficient (BCC, units: kg MJ −1 ). The PrePost and Pooled approaches yielded similar results at Las Conchas, but at Pole Creek insufficient pre-fire field data resulted in erroneous fuel consumption estimates outside the fire perimeter using the PrePost models. These results demonstrated that pre-fire field data were less important for these models than having field data which represent the full range of fuel conditions likely to exist across the landscape. Estimated total biomass consumed for the PrePost, Pooled, and Global models were 226 Gg, 224 Gg, and 224 Gg at Las Conchas, and 581 Gg, 713 Gg, and 552 Gg at Pole Creek. Comparisons between estimated ΔTF and FRE yielded an average BCC for both fires of 0.367 (s.d. ± 0.049) kg MJ −1 based on pixels with at least five MODIS observations. Both higher MODIS observations per pixel and accounting for canopy occlusion of FRE improved the relationship between ΔTF and MODIS-FRE. This study suggested a practical modelling approach for future efforts using only post-fire field observations and quantified a landscape-scale relationship between MODIS-derived FRE and fine-scale fuel consumption consistent with prior experiments.

New Mexico, Oregon↗

USGS2009

Method development for analysis of urban dust using scanning electron microscopy with energy dispersive x-ray spectrometry to detect the possible presence of world trade center dust constituents

The collapse of the World Trade Center Towers on September 11, 2001, sent dust and debris across much of Manhattan and in the surrounding areas. Indoor and outdoor dust samples were collected and characterized by U.S. Geological Survey (USGS) scientists using scanning electron microscopy with energy-dispersive spectrometry (SEM/EDS). From this characterization, the U.S. Environmental Protection Agency and USGS developed a particulate screening method to determine the presence of residual World Trade Center dust in the indoor environment using slag wool as a primary "signature". The method describes a procedure that includes splitting, ashing, and sieving of collected dust. From one split, a 10 mg/mL dust/ isopropanol suspension was prepared and 10-30 ??L aliquots of the suspension placed on an SEM substrate. Analyses were performed using SEM/EDS manual point counting for slag wool fibers. Poisson regression was used to identify some of the sources of uncertainty, which are directly related to the small number of fibers present on each sample stub. Preliminary results indicate that the procedure is promising for screening urban background dust for the presence of WTC dust. Consistent sample preparation of reference materials and samples must be performed by each laboratory wishing to use this method to obtain meaningful and accurate results. ?? 2009 American Chemical Society.

Environmental Science & Technology↗

USGS2018

Method to characterize inorganic particulates in lung tissue biopsies using field emission scanning electron microscopy

Humans accumulate large numbers of inorganic particles in their lungs over a lifetime. Whether this causes or contributes to debilitating disease over a normal lifespan depends on the type and concentration of the particles. We developed and tested a protocol for in situ characterization of the types and distribution of inorganic particles in biopsied lung tissue from three human groups using field emission scanning electron microscopy (FE-SEM) combined with energy dispersive spectroscopy (EDS). Many distinct particle types were recognized among the 13 000 particles analyzed. Silica, feldspars, clays, titanium dioxides, iron oxides and phosphates were the most common constituents in all samples. Particles were classified into three general groups: endogenous , which form naturally in the body; exogenic particles, natural earth materials; and anthropogenic particles, attributed to industrial sources. These in situ results were compared with those using conventional sodium hypochlorite tissue digestion and particle filtration. With the exception of clays and phosphates, the relative abundances of most common particle types were similar in both approaches. Nonetheless, the digestion/filtration method was determined to alter the texture and relative abundances of some particle types. SEM/EDS analysis of digestion filters could be automated in contrast to the more time intensive in situ analyses.

Toxicology Mechanisms and Methods↗

USGS2015

Estimating sturgeon abundance in the Carolinas using side-scan sonar

Sturgeons (Acipenseridae) are one of the most threatened taxa worldwide, including species in North Carolina and South Carolina. Populations of Atlantic Sturgeon Acipenser oxyrinchus in the Carolinas have been significantly reduced from historical levels by a combination of intense fishing and habitat loss. There is a need for estimates of current abundance, to describe status, and for estimates of historical abundance in order to provide realistic recovery goals. In this study we used N -mixture and distance models with data acquired from side-scan sonar surveys to estimate abundance of sturgeon in six major sturgeon rivers in North Carolina and South Carolina. Estimated abundances of sturgeon greater than 1 m TL in the Carolina distinct population segment (DPS) were 2,031 using the count model and 1,912 via the distance model. The Pee Dee River had the highest overall abundance of any river at 1,944 (count model) or 1,823 (distance model). These estimates do not account for sturgeon less than 1 m TL or occurring in riverine reaches not surveyed or in marine waters. Comparing the two models, the N -mixture model produced similar estimates using less data than the distance model with only a slight reduction of estimated precision.

Marine and Coastal Fisheries: Dynamics, Management↗

USGS1984

Side-scan sonar assessment of gray whale feeding in the Bering Sea

Side-scan sonar was used to map and measure feeding pits of the California gray whale over 22,000 square kilometers of the northeastern Bering Sea floor. The distribution of pits, feeding whales, ampeliscid amphipods (whale prey), and a fine-sand substrate bearing the amphipods were all closely correlated. The central Chirikov Basin and nearshore areas of Saint Lawrence Island supply at least 6.5 percent of the total gray whale food resource in summer. While feeding, the whales resuspend at least 1.2 × 10 8 cubic meters of sediment annually; this significantly affects the geology and biology of the region.

Alaska↗

USGS1968

Aquilapollenites: Fossil pollen as seen under the scanning electron microscope

Photographs of a Late Cretaceous species of Aquilapollenites illustrate the usefulness of the scanning electron microscope (SEM) for the study of fossil pollen . The SEM has the advantages of great depth of focus and wide range of magnification; using present techniques, its use for the study of unsectioned specimens is limited to the observation of surface detail.

Geological Society of America Bulletin↗

USGS2025

Combining acoustic telemetry and side-scan sonar to estimate abundance of endangered shortnose sturgeon in the Hudson River, New York

For endangered shortnose sturgeon (Acipenser brevirostrum), the ability to estimate and monitor population size is critical for tracking species’ recovery. Yet, contemporary abundance estimates have not been completed for many shortnose sturgeon populations, largely owing to the difficulty in using traditional abundance estimators for sturgeons. Here, we estimate the adult shortnose sturgeon population size of the Hudson River, NY by integrating data from two largely passive sampling methods – acoustic telemetry and side-scan sonar – into a Bayesian hierarchical model of abundance. We estimated the adult abundance to be 69,798 individuals (95% CI = 9,207-185,666), making the Hudson River the largest extant shortnose sturgeon population. Despite this, the population remains vulnerable to localized disturbances, as over 40% of the population congregated in a small overwintering habitat that coincides with an area of high anthropogenic activity. Accordingly, recurrent demographic surveys may be beneficial for gaining insight into the relative effects of anthropogenic and naturally stochastic processes shaping shortnose sturgeon demography. Our modeling framework provides a relatively low-cost alternative for future demographic monitoring of species of conservation concern.

New York↗

USGS2006

An exploratory method to detect tephras from quantitative XRD scans: Examples from Iceland and east Greenland marine sediments

Tephras, mainly from Iceland, are becoming increasingly important in interpreting leads and lags in the Holocene climate system across NW Europe. Here we demonstrate that Quantitative Phase Analysis of x-ray diffractograms of the < 2 mm of marine sediment fraction (ie, sand, silt and clay) from Iceland and East Greenland can detect peaks in volcanic glass concentrations (weight%) even though discrete tephra layers are not visible; thus it provides a rapid overview of the probable location of volcanic glass within sediment sequences. Experiments in spiking samples from Baffin Bay and an artificial mixture of minerals with known weight% fractions of an Icelandic tephra (Hekla 4) demonstrate a significant correlation (r2 = 0.92 and 0.97) between known and estimated weight percentages, although the slope of the measured to observed weight% is around 0.65 and not 1.0 as expected. In core B997-321PC off North Iceland we identify tephras from point counting in the > 150 um fraction and identify these same peaks in XRD scans - two of these correlate geochemically and chronologically with Hekla 1104 and 3. At a distal site to the WNW of Iceland, on the East Greenland margin (core MD99-2317), the weight% of volcanic glass reaches values of 11% at about the time of the Saksunarvatn tephra. The XRD method identifies the presence of volcanic glass but not its elemental composition; hence it will assist in focusing attention on specific sections of sediment cores for subsequent geochemical fingerprinting of tephras. ?? 2006 SAGE Publications.

Holocene↗

USGS1987

Sedimentary processes on the northwestern Iberian continental margin viewed by long-range side-scan sonar and seismic data

The effects of an eastern boundary current in the North Atlantic have been mapped from about 39° north latitude along the Iberian margin to as far north as 43°30 north latitude at the western margin of Galicia Bank. The geostrophic current has produced sediment drifts that are covered with bedforms. The sediment drifts are difficult to detect on Gloria long-range side-scan sonar data but are easily resolved on seismic-reflection records as anomalously thick accumulations of sediment banked against either buried or outcropping basement highs. The bedforms ornamenting the drift surfaces were subdivided into 1,000-m water-depth intervals, and their dimensions were tabulated. There are few bedforms in water depths less han 2,000 m, but from depths between 2,000 and 4,000 m they are numerous and have a mean wavelength of 695 m. Bedforms from depths greater than 4,000 m have a mean wavelength of 999 m. The different wavelengths from different water depths suggest two distinct and separated boundary flows. The wave heights of all bedforms found in water depths greater than 2,000 m are less than 10 m. In order to investigate the continuity of sediment drifting through geological time, the stratigraphic section drilled at DSDP Site 398 was reinterpreted and, using seismic-reflection profiles, was traced throughout the northern Iberian margin. Together, the lithostratigraphic and seismic data indicate that sediment drifting developed along this margin in the Eocene. The lithofacies of the Eocene section is t e oldest to have numerous layers of sand and silt. An unconformity separates the Eocene section from the latest Miocene-Pliocene section. The unconformity is interpreted to be the result of the initial pulses of Mediterranean outflow that followed the Messinian desiccation events. A second period of sediment drifting commenced during the Pliocene once the Mediterranean basin filled and the flow out of the Strait of Gibraltar resumed.

Journal of Sedimentary Petrology↗

USGS2024

Scanning electron microscopy of clays and clay minerals

The scanning electron microscope (SEM) proves to be ideally suited for studying the configuration, texture, and fabric of clay samples. Growth mechanics of crystalline units—interpenetration and interlocking of crystallites, crystal habits, twinning, helical growth, and topotaxis—also are uniquely revealed by the SEM. Authigenic kaolins make up the bulk of the examples because their larger crystallite size, better crystallinity, and open texture make them more suited to examination by the SEM than most other clay mineral types.

Clays and Clay Minerals↗

USGS2017

Analysis of artificially matured shales with confocal laser scanning raman microscopy: Applications to organic matter characterization

Raman spectroscopy has been suggested as a method for characterizing the thermal maturity of rocks. The literature contains many empirical correlations between thermal maturity proxies, such as vitrinite reflectance (V Ro ) and pyrolysis-T max , with spectral metrics such as Raman peak-widths, peak-center positions, peak-areas and all manner of differences and ratios of these parameters. However, while these correlations may be convincing for small data sets from limited sample series, broader application of these metrics to disparate and heterogeneous samples proves difficult and there remains no consensus. In this extended abstract, Raman spectroscopy is introduced and the history of Raman analysis of carbonaceous material is briefly outlined, highlighting some of the latent difficulties and potential sources of bias. We suggest the organization of a community working group to establish terminology, guidelines, procedures and standards necessary for the successful development of this technique to characterize organic matter in an accessible, unbiased, and reproducible manner. For the present multi-phase study, immature shale samples from the Bakken and Duvernay formations were subjected to hydrous pyrolysis for 72 hours at temperatures from 280°C to 360°C. Rock residues were mounted and polished for analysis via confocal laser-scanning Raman microscopy and reflectance. The maturation series from the Bakken was randomized for the Phase-I single-blind study to be presented at this conference. For the Phase-II study, solid bitumen reflectance (B Ro ) values for the Duvernay series will be known. Multiple hyperspectral maps were collected from each Bakken sample, with each map consisting of a single diffraction-limited spot-size spectrum per 1 µm 2 in rectangular areas several hundred micrometers on a side. Initial attempts at using basic spectral metrics on small numbers of hand-selected spectra to sort the blind series produced inconclusive results: any number of possible correlations could be found. In an improved approach, the statistics of the full spectral datasets were leveraged to: 1) objectively identify organic carbon types (OCTs) in a given map based on Raman and fluorescence spectral characteristics, 2) identify those OCTs in other maps from the same sample and determine if the heterogeneity of the sample has been adequately characterized, and 3) identify the same OCTs in maps from other samples in the maturation series. In ongoing work, our goals are to: 1) use these analyses of the blind series to develop a hypothesis for a correlation to maturation, 2) test the hypothesis by applying the same analyses to the known Duvernay series (in Phase-II), 3) if necessary refine the hypothesis based on observations from the Duvernay analysis, and 4) finally reveal the true order of the Bakken series to verify if the hypothesized correlation accurately predicts the maturity order of the samples. In this document, we share progress to date. The analysis of one area of interest is detailed showing the differentiation of two OCTs based on Raman and fluorescence spectral features, including the use of 2-factor histograms, Principle Components Analysis (PCA), and Nonlinear Iterative Peak Fitting (NIPF).

Conference Paper↗

USGS1989

Side-scan sonar mapping of lake trout spawning habitat in northern Lake Michigan

Native stocks of lake trout Salvelinus namaycush were virtually or completely extirpated from the lower four Great Lakes by the early 1960s. The failure of early attempts to reestablish self-sustaining populations of lake trout was attributed partly to the practice of stocking hatcheryreared juveniles at locations and over substrates that had not been used in the past for spawning by native fish. Subsequent attempts to improve the selection of stocking locations were impeded by the lack of reliable information on the distribution of substrates on historical spawning grounds. Here we demonstrate the potential of side-scan sonar to substantially expand the data base needed to pinpoint the location of substrates where lake trout eggs, fry, or juveniles could be stocked to maximize survival and help ensure that survivors returning to spawn would encounter suitable substrates. We also describe the substrates and bathymetry of large areas on historical lake trout spawning grounds in the Fox Island Lake Trout Sanctuary in northern Lake Michigan. These areas could be used to support a contemporary self-sustaining lake trout population in the sanctuary and perhaps also in adjacent waters.

Great Lakes↗

USGS2016

Modeling streamflow from coupled airborne laser scanning and acoustic Doppler current profiler data

The rating curve enables the translation of water depth into stream discharge through a reference cross-section. This study investigates coupling national scale airborne laser scanning (ALS) and acoustic Doppler current profiler (ADCP) bathymetric survey data for generating stream rating curves. A digital terrain model was defined from these data and applied in a physically based 1-D hydraulic model to generate rating curves for a regularly monitored location in northern Sweden. Analysis of the ALS data showed that overestimation of the streambank elevation could be adjusted with a root mean square error (RMSE) block adjustment using a higher accuracy manual topographic survey. The results of our study demonstrate that the rating curve generated from the vertically corrected ALS data combined with ADCP data had lower errors (RMSE = 0.79 m 3 /s) than the empirical rating curve (RMSE = 1.13 m 3 /s) when compared to streamflow measurements. We consider these findings encouraging as hydrometric agencies can potentially leverage national-scale ALS and ADCP instrumentation to reduce the cost and effort required for maintaining and establishing rating curves at gauging station sites similar to the Röån River.

Hydrology Research↗

USGS2017

Scanning and georeferencing historical USGS quadrangles

The U.S. Geological Survey (USGS) National Geospatial Program is scanning published USGS 1:250,000-scale and larger topographic maps printed between 1884, the inception of the topographic mapping program, and 2006. The goal of this project, which began publishing the Historical Topographic Map Collection in 2011, is to provide access to a digital repository of USGS topographic maps that is available to the public at no cost. For more than 125 years, USGS topographic maps have accurately portrayed the complex geography of the Nation. The USGS is the Nation’s largest producer of traditional topographic maps, and, prior to 2006, USGS topographic maps were created using traditional cartographic methods and printed using a lithographic process. The next generation of topographic maps, US Topo, is being released by the USGS in digital form, and newer technologies make it possible to also deliver historical maps in the same electronic format that is more publicly accessible.

Fact Sheet↗

USGS2010

Examination of Libby, Montana, Fill Material for Background Levels of Amphibole from the Rainy Creek Complex Using Scanning Electron Microscopy and X-Ray Microanalysis

Natural background levels of Libby-type amphibole in the sediment of the Libby valley in Montana have not, up to this point, been determined. The purpose of this report is to provide the preliminary findings of a study designed by both the U.S. Geological Survey and the U.S. Environmental Protection Agency and performed by the U.S. Geological Survey. The study worked to constrain the natural background levels of fibrous amphiboles potentially derived from the nearby Rainy Creek Complex. The material selected for this study was sampled from three localities, two of which are active open-pit sand and gravel mines. Seventy samples were collected in total and examined using a scanning electron microscope equipped with an energy dispersive x-ray spectrometer. All samples contained varying amounts of feldspars, ilmenite, magnetite, quartz, clay minerals, pyroxene minerals, and non-fibrous amphiboles such as tremolite, actinolite, and magnesiohornblende. Of the 70 samples collected, only three had detectable levels of fibrous amphiboles compatible with those found in the rainy creek complex. The maximum concentration, identified here, of the amphiboles potentially from the Rainy Creek Complex is 0.083 percent by weight.

Open-File Report↗

USGS2022

Results of automated scanning electron microscope (SEM) analyses of rock and stream sediment samples from the Taurus porphyry copper deposit area, Tanacross quadrangle, eastern Alaska

Numerous porphyry copper-molybdenum-gold and epithermal deposits define a belt that extends from Eastern Alaska to western Yukon, Canada. An orientation study conducted near the Taurus porphyry deposit was designed to test methods that require minimal sample collection, preparation, and analytical time to determine the viability of indicator mineral studies as a reconnaissance exploration method. Bulk stream sediments and altered and mineralized rocks were sieved to the 0.105−0.25 millimeter fraction (+140, −60 mesh) and passed over a shaking table to create a moderate to heavy mineral separate that was mounted in epoxy and subsequently analyzed using automated scanning electron microscope (SEM) techniques. Seven polished thin sections of core were also analyzed. Among the advantages of automated SEM techniques compared to visual mineral identification are that thousands of grains can be rapidly identified in each sample (about 1 hour per sample) and small quantities of indicator minerals that may be missed during traditional visual analyses can be detected. Automated SEM analyses of stream sediment and rock samples show that specific minerals (chalcopyrite, bornite, and jarosite) are indicators of potential mineralized areas. Svanbergite, an aluminum sulfate phosphate mineral, was identified in mineralized rocks and in nearly all stream sediment samples (up to 9 kilometers) downstream from the Taurus and other porphyry occurrences but not epithermal occurrences. It was not identified in areas with no known mineralization and thus it is possibly one of the best indicator minerals for porphyry copper (+/- molybdenum, gold) occurrences.

Alaska↗

USGS1998

MORPH-I (Ver 1.0) a software package for the analysis of scanning electron micrograph (binary formatted) images for the assessment of the fractal dimension of enclosed pore surfaces

MORPH-I is a set of C-language computer programs for the IBM PC and compatible minicomputers. The programs in MORPH-I are used for the fractal analysis of scanning electron microscope and electron microprobe images of pore profiles exposed in cross-section. The program isolates and traces the cross-sectional profiles of exposed pores and computes the Richardson fractal dimension for each pore. Other programs in the set provide for image calibration, display, and statistical analysis of the computed dimensions for highly complex porous materials. Requirements: IBM PC or compatible; minimum 640 K RAM; mathcoprocessor; SVGA graphics board providing mode 103 display.

Open-File Report↗

USGS2023

Scanning electron microscope images of sand and silt from the early MIS4–MIS3 Roxana Silt, Phillips Bayou, Arkansas

The age and source of the late Pleistocene Roxana Silt in the Mississippi Valley have been studied since the middle 1800s. Published age and paleoenvironmental data for the Roxana Silt in the Mississippi Valley show that deposition occurred from late marine isotope stage 5 (MIS5) through late marine isotope stage 3 (MIS3) (80–30 kilo-annum [ka]), when the warm to hot interglacial climate of early to middle MIS5 (about 130 to about 80 ka) was transitioning to a considerably cooler and wetter climate. Scanning electron microscopy/energy dispersive X-ray (SEM/EDS) analysis of silt and sand grains from the Roxana Silt exposed in an abandoned borrow pit near Phillips Bayou, Arkansas, was performed as part of a 1990s study of late middle and late Pleistocene loess in the unglaciated lower Mississippi Valley. Results from that study were summarized in 1990s publications, but the data for sand and silt grain morphology and mineralogy were not published. Some of the SEM/EDS analyses of the Roxana Silt from that late 1990s study are presented in this report. Combined with previously published chronostratigraphic and pedostratigraphic data for the Roxana Silt at Phillips Bayou, the SEM/EDS data indicate some degree of syndepositional weathering and pedogenic alteration during and after gradual eolian deposition in late marine isotope stage 4 (MIS4) and MIS3 (about 60 to about 30 ka). Results from the SEM/EDS analyses support previously published paleoclimate interpretations indicating that at least as far south as northern Mississippi, the climate of the Mississippi Valley in MIS4 and MIS3 (about 70 to about 30 ka) was cool to cold and humid to wet.

Arkansas↗