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USGS1994

Geochemical soil sampling for deeply-buried mineralized breccia pipes, northwestern Arizona

Thousands of solution-collapse breccia pipes crop out in the canyons and on the plateaus of northwestern Arizona; some host high-grade uranium deposits. The mineralized pipes are enriched in Ag, As, Ba, Co, Cu, Mo, Ni, Pb, Sb, Se, V and Zn. These breccia pipes formed as sedimentary strata collapsed into solution caverns within the underlying Mississippian Redwall Limestone. A typical pipe is approximately 100 m (300 ft) in diameter and extends upward from the Redwall Limestone as much as 1000 m (3000 ft). Unmineralized gypsum and limestone collapses rooted in the Lower Permian Kaibab Limestone or Toroweap Formation also occur throughout this area. Hence, development of geochemical tools that can distinguish these unmineralized collapse structures, as well as unmineralized breccia pipes, from mineralized breccia pipes could significantly reduce drilling costs for these orebodies commonly buried 300–360 m (1000–1200 ft) below the plateau surface. Design and interpretation of soil sampling surveys over breccia pipes are plagued with several complications. (1) The plateau-capping Kaibab Limestone and Moenkopi Formation are made up of diverse lithologies. Thus, because different breccia pipes are capped by different lithologies, each pipe needs to be treated as a separate geochemical survey with its own background samples. (2) Ascertaining true background is difficult because of uncertainties in locations of poorly-exposed collapse cones and ring fracture zones that surround the pipes. Soil geochemical surveys were completed on 50 collapse structures, three of which are known mineralized breccia pipes. Each collapse structure was treated as an independent geochemical survey. Geochemical data from each collapse feature were plotted on single-element geochemical maps and processed by multivariate factor analysis. To contrast the results between geochemical surveys (collapse structures), a means of quantifying the anomalousness of elements at each site was developed. This degree of anomalousness, named the “correlation value”, was used to rank collapse features by their potential to overlie a deeply-buried mineralized breccia pipe. Soil geochemical results from the three mineralized breccia pipes (the only three of the 50 that had previously been drilled) show that: (1) Soils above the SBF pipe contain significant enrichment of Ag, Al, As, Ba, Ga, K, La, Mo, Nd, Ni, Pb, Sc, Th, U and Zn, and depletion in Ca, Mg and Sr, in contrast to soils outside the topographic and structural rim; (2) Soils over the inner treeless zone of the Canyon pipe show Mo and Pb enrichment anf As and Ga depletion, in contrast to soils from the surrounding forest; and (3) The soil survey of the Mohawk Canyon pipe was a failure because of the rocky terrane and lack of a B soil horizon, or because the pipe plunges. At least 11 of the 47 other collapse structures studied contain anomalous soil enrichments similar to the SBF uranium ore-bearing pipe, and thus have good potential as exploration targets for uranium. One of these 11, #1102, does contain surface mineralized rock. These surveys suggest that soil geochemical sampling is a useful tool for the recognition of many collapse structures with underlying ore-bearing breccia pipes.

Arizona↗

USGS2014

Depletion of eugenol residues from the skin-on fillet tissue of rainbow trout exposed to 14C-labeled eugenol

The U.S. is lagging in access to an approved immediate-release sedative, i.e. a compound that can be safely and effectively used to sedate fish and has no withdrawal period. AQUI-S® 20E (10% active ingredient, eugenol) is under investigation as an immediate-release sedative for freshwater finfish. Because of its investigational status, data are needed to characterize the depletion, distribution, and identity of AQUI-S® 20E residues in fillet tissue. Rainbow trout ( Oncorhynchus mykiss ) were exposed to uniformly ring labeled 14 C-eugenol at a nominal concentration of 10 mg/L for 60 min in 18 °C water. Fish (n = 6) were sampled immediately after the exposure (0 min) then at 30, 60, 120, and 240 min. Eugenol concentrations and characterization of 14 C residues in the fillet tissue were determined by high pressure liquid chromatography and flow-through liquid scintillation counting techniques. Total 14 C-residue burdens in fillet tissue were determined by tissue oxidation and static liquid scintillation counting techniques. Maximum eugenol and 14 C-eugenol equivalent residue concentrations in the fillet tissue were measured immediately after the exposure (44.5 and 38.8 μg/g, respectively). Eugenol was the primary 14 C-residue (> 90% of all 14 C-residues) in extracts from fillet tissue taken from fish sampled immediately after the exposure (0 min) and from fish sampled at 30 and 60 min after the exposure. The depletion of 14 C-eugenol residues from the fillet tissue was rapid (t 1/2 = 26.25 min) after transferring the exposed fish to fresh flowing water.

Aquaculture↗

USGS2016

Chemical abrasion-SIMS (CA-SIMS) U-Pb dating of zircon from the late Eocene Caetano caldera, Nevada

Zircon geochronology is a critical tool for establishing geologic ages and time scales of processes in the Earth's crust. However, for zircons compromised by open system behavior, achieving robust dates can be difficult. Chemical abrasion (CA) is a routine step prior to thermal ionization mass spectrometry (TIMS) dating of zircon to remove radiation-damaged parts of grains that may have experienced open system behavior and loss of radiogenic Pb. While this technique has been shown to improve the accuracy and precision of TIMS dating, its application to high-spatial resolution dating methods, such as secondary ion mass spectrometry (SIMS), is relatively uncommon. In our efforts to U-Pb date zircons from the late Eocene Caetano caldera by SIMS (SHRIMP-RG: sensitive high resolution ion microprobe, reverse geometry), some grains yielded anomalously young U-Pb ages that implicated Pb-loss and motivated us to investigate with a comparative CA and non-CA dating study. We present CA and non-CA 206 Pb/ 238 U ages and trace elements determined by SHRIMP-RG for zircons from three Caetano samples (Caetano Tuff, Redrock Canyon porphyry, and a silicic ring-fracture intrusion) and for R33 and TEMORA-2 reference zircons. We find that non-CA Caetano zircons have weighted mean or bimodal U-Pb ages that are 2–4% younger than CA zircons for the same samples. CA Caetano zircons have mean U-Pb ages that are 0.4–0.6 Myr older than the 40 Ar/ 39 Ar sanidine eruption age (34.00 ± 0.03 Ma; error-weighted mean, 2σ), whereas non-CA zircons have ages that are 0.7–1.3 Myr younger. U-Pb ages do not correlate with U (~ 100–800 ppm), Th (~ 50–300 ppm) or any other measured zircon trace elements (Y, Hf, REE), and CA and non-CA Caetano zircons define identical trace element ranges. No statistically significant difference in U-Pb age is observed for CA versus non-CA R33 or TEMORA-2 zircons. Optical profiler measurements of ion microprobe pits demonstrate consistent depths of ~ 1.6 μm for CA and non-CA Caetano, R33 and TEMORA-2 zircons, and do not indicate variations in secondary ion sputtering rates due to chemical or structural changes from the CA treatment. Our new data underscore the potential for cryptic Pb-loss to go unrecognized in other geologically young magmatic centers that do not have zircons with high U, statistically discordant isotope ratios, high common Pb, or metamict textures.

Nevada↗

USGS2013

Polybrominated diphenyl ether metabolism in field collected fish from the Gila River, Arizona, USA-Levels, possible sources, and patterns

Polybrominated diphenyl ethers (PBDEs) were determined in fish collected from the Gila River, Arizona, a tributary of the Colorado River in the lower part of the Colorado River Basin. Fish samples were collected at sites on the Gila River downstream from Hayden, Phoenix, and Arlington, Arizona in late summer 2003. The Gila River is ephemeral upstream of the Phoenix urban area due to dams and irrigation projects and has limited perennial flow downstream of Phoenix due to wastewater and irrigation return flows. Fifty PBDE congeners were analyzed by high resolution gas chromatography/high resolution mass spectrometry using labeled surrogate standards in composite samples of male and female common carp ( Cyrpinus carpio ), largemouth bass ( Micropterus salmoides ) and channel catfish ( Ictalurus punctatus ). The predominant PBDE congeners detected and quantified were 47, 100, 153, 49, 28, and 17. Concentrations of total PBDEs in these fish ranged from 1.4 to 12700 ng g -1 wet weight, which are some of the highest concentrations reported in fish from the United States. Differences in metabolism of several PBDE congeners by carp is clear at the Phoenix site; congeners with at least one ring of 2,4,5-substitution are preferentially metabolized as are congeners with 2,3,4-substitution.

Arizona↗

USGS2011

Chemical structures of coal lithotypes before and after CO2 adsorption as investigated by advanced solid-state 13C nuclear magnetic resonance spectroscopy

Four lithotypes (vitrain, bright clarain, clarain, and fusain) of a high volatile bituminous Springfield Coal from the Illinois Basin were characterized using advanced solid-state 13 C nuclear magnetic resonance (NMR) spectroscopy. The NMR techniques included quantitative direct polarization/magic angle spinning (DP/MAS), cross polarization/total sideband suppression (CP/TOSS), dipolar dephasing, CH n selection, and recoupled C–H long-range dipolar dephasing techniques. The lithotypes that experienced high-pressure CO 2 adsorption isotherm analysis were also analyzed to determine possible changes in coal structure as a result of CO 2 saturation at high pressure and subsequent evacuation. The main carbon functionalities present in original vitrain, bright clarain, clarain and fusain were aromatic carbons (65.9%–86.1%), nonpolar alkyl groups (9.0%–28.9%), and aromatic C–O carbons (4.1%–9.5%). Among these lithotypes, aromaticity increased in the order of clarain, bright clarain, vitrain, and fusain, whereas the fraction of alkyl carbons decreased in the same order. Fusain was distinct from other three lithotypes in respect to its highest aromatic composition (86.1%) and remarkably small fraction of alkyl carbons (11.0%). The aromatic cluster size in fusain was larger than that in bright clarain. The lithotypes studied responded differently to high pressure CO 2 saturation. After exposure to high pressure CO 2 , vitrain and fusain showed a decrease in aromaticity but an increase in the fraction of alkyl carbons, whereas bright clarain and clarain displayed an increase in aromaticity but a decrease in the fraction of alkyl carbons. Aromatic fused-rings were larger for bright clarain but smaller for fusain in the post-CO 2 adsorption samples compared to the original lithotypes. These observations suggested chemical CO 2 –coal interactions at high pressure and the selectivity of lithotypes in response to CO 2 adsorption.

International Journal of Coal Geology↗

USGS2012

Compression map, functional groups and fossilization: A chemometric approach (Pennsylvanian neuropteroid foliage, Canada)

Nearly all of the spectrochemical studies involving Carboniferous foliage of seed-ferns are based on a limited number of pinnules, mainly compressions. In contrast, in this paper we illustrate working with a larger pinnate segment, i.e., a 22-cm long neuropteroid specimen, compression-preserved with cuticle, the compression map. The objective is to study preservation variability on a larger scale, where observation of transparency/opacity of constituent pinnules is used as a first approximation for assessing the degree of pinnule coalification/fossilization. Spectrochemical methods by Fourier transform infrared spectrometry furnish semi-quantitative data for principal component analysis. The compression map shows a high degree of preservation variability, which ranges from comparatively more coalified pinnules to less coalified pinnules that resemble fossilized-cuticles, noting that the pinnule midveins are preserved more like fossilized-cuticles. A general overall trend of coalified pinnules towards fossilized-cuticles, i.e., variable chemistry, is inferred from the semi-quantitative FTIR data as higher contents of aromatic compounds occur in the visually more opaque upper location of the compression map. The latter also shows a higher condensation of the aromatic nuclei along with some variation in both ring size and degree of aromatic substitution. From principal component analysis we infer correspondence between transparency/opacity observation and chemical information which correlate with varying degree to fossilization/coalification among pinnules.

Nova Scotia↗

USGS2018

A multi-species synthesis of satellite telemetry data in the Pacific Arctic (1987–2015): Overlap of marine mammal distributions and core use areas

We collated available satellite telemetry data for six species of ice-associated marine mammals in the Pacific Arctic: ringed seals ( Pusa hispida ; n = 118), bearded seals( Erignathus barbatus, n = 51), spotted seals ( Phoca largha , n = 72), Pacific walruses ( Odobenus rosmarus divergens, n = 389); bowhead whales ( Balaena mysticetus , n = 46), and five Arctic and sub-arctic stocks of beluga whales ( Delphinapterus leucas , n = 103). We also included one seasonal resident, eastern North Pacific gray whales ( Eschrichtius robustus , n = 12). This review summarized the distribution of daily locations from satellite-linked transmitters during two analysis periods, summer (May–November) and winter (December–April), and then examined the overlap among species. Six multi-species core use areas were identified during the summer period: 1) Chukotka/Bering Strait; 2) Norton Sound; 3) Kotzebue Sound; 4) the northeastern Chukchi Sea; 5) Mackenzie River Delta/Amundsen Gulf; and 6) Viscount Melville Sound. During the winter period, we identified four multi-species core use areas: 1) Anadyr Gulf/Strait; 2) central Bering Sea; 3) Nunivak Island; and 4) Bristol Bay. During the summer period, four of the six areas were centered on the greater Bering Strait region and the northwestern coast of Alaska and included most of the species we examined. The two remaining summer areas were in the western Canadian Arctic and were largely defined by the seasonal presence of Bering-Chukchi-Beaufort stock bowhead whales and Eastern Beaufort Sea stock beluga whales, whose distribution overlapped during both summer and winter periods. During the winter period, the main multi-species core use area was located near the Gulf of Anadyr and extended northwards through Anadyr and Bering Straits. This area is contained within the Bering Sea “green belt”, an area of enhanced primary and secondary productivity in the Bering Sea. We also described available telemetry data and where they can be found as of 2017. These data are important for understanding ice-associated marine mammal movements and habitat use in the Pacific Arctic and should be archived, with appropriate metadata, to ensure they are available for future retrospective analyses.

Deep Sea Research Part II: Topical Studies in Ocea↗

USGS2025

Shear surface undulations modulate clayey gouge strength and contribute to divergent landslide acceleration

Landslides display a spectrum of speeds for incompletely known reasons. Sliding occurs along slickensided undulatory shear surfaces within boundary shear gouge. Laboratory tests reveal that gouge shear strength generally decreases with finite cumulative displacement during relatively rapid failure and may increase or decrease with increasing shear rate; these behaviors can result in accelerating or decelerating landslide motion, which significantly affects consequent hazards. However, mechanisms responsible for such behaviors are poorly understood. We performed advanced ring shear strength testing that revealed such variable strength of a landslide near Oso, Washington, USA. We hypothesized that millimeter-scale undulations along shear surfaces caused the strength variability by imparting shear strength but while also modifying stresses that locally increase and decrease the typically considered particle-scale shear strength. We tested our hypotheses in the laboratory and with finite element soil deformation modeling. Lab results suggest that undulations contribute strength that decays with finite cumulative displacement. Modeling similarly reveals this, and that rapid shearing across undulations locally reduces effective normal stress by persistently elevating pore-water pressure and causing dilation. Consequent effects on strength differ by material with granular-rich, high-friction gouge losing strength and clay-rich, low-friction gouge losing little or gaining strength as shear rates increase. Ample testing by others reveals similar patterns. Hence, the propensity for gouge-controlled accelerating or decelerating failure may be estimated from simple index tests. Our findings on the effects of undulations reveal previously unknown mechanisms that may help to explain why some landslides reactivate catastrophically while others do not.

Washington↗

USGS2007

Empirical evaluation of decision support systems: Needs, definitions, potential methods, and an example pertaining to waterfowl management

Decision support systems are often not empirically evaluated, especially the underlying modelling components. This can be attributed to such systems necessarily being designed to handle complex and poorly structured problems and decision making. Nonetheless, evaluation is critical and should be focused on empirical testing whenever possible. Verification and validation, in combination, comprise such evaluation. Verification is ensuring that the system is internally complete, coherent, and logical from a modelling and programming perspective. Validation is examining whether the system is realistic and useful to the user or decision maker, and should answer the question: “Was the system successful at addressing its intended purpose?” A rich literature exists on verification and validation of expert systems and other artificial intelligence methods; however, no single evaluation methodology has emerged as preeminent. At least five approaches to validation are feasible. First, under some conditions, decision support system performance can be tested against a preselected gold standard. Second, real-time and historic data sets can be used for comparison with simulated output. Third, panels of experts can be judiciously used, but often are not an option in some ecological domains. Fourth, sensitivity analysis of system outputs in relation to inputs can be informative. Fifth, when validation of a complete system is impossible, examining major components can be substituted, recognizing the potential pitfalls. I provide an example of evaluation of a decision support system for trumpeter swan ( Cygnus buccinator ) management that I developed using interacting intelligent agents, expert systems, and a queuing system. Predicted swan distributions over a 13-year period were assessed against observed numbers. Population survey numbers and banding (ringing) studies may provide long term data useful in empirical evaluation of decision support.

Environmental Modelling and Software↗

USGS2012

Morphological and chemical evidence of stromatolitic deposits in the 2.75 Ga Carajás banded iron formation, Brazil

We describe evidence of biogenicity in the morphology and carbon content of well-preserved, Neoarchean samples of banded iron formation (BIF) from Carajás, Brazil. Silica-rich BIF layers contain translucent ellipsoidal or trapezoidal structures (∼5–10 μm diameter) composed of silica, hematite, and kerogen, which are arranged in larger ring-like forms (rosettes). Stable carbon isotope analysis yields a δ 13 C value of −24.5‰ indicating that the contained carbon is likely biogenic. Raman and SEM analyses, as well as wavelength-dispersive X-ray elemental maps, show kerogen inside the rosette forms. Within the iron-rich BIF layers, tubular structures (0.5–5 μm) were observed between hematite granules and blades. Kerogen and kaolinite are present in these structures. Both the rosettes and the tubular structures resemble morphologies that are characteristic of some bacterial species. We hypothesize that the Carajás BIFs originated as biomats formed by one or more species that over time produced large stromatolitic structures. The rosettes and the tubular structures, associated with chert-rich and iron-rich BIF layers, respectively, may represent two different species, or perhaps, two phases of a bacterium life cycle. For example, some modern myxobacteria exhibit similar morphologies in their resting and vegetative stages. Fe(III) precipitation may have occurred by contact of Fe(II) with bacterial slime, leading to oxidation by chemical reactions with exposed polysaccharide hydroxyl and carboxyl groups. The Fe(III) would then have been available for use as a source of energy in a dissimilatory iron reduction type of metabolism. Organic carbon input presumably came from primary producers (not necessarily aerobic) within the local water column, perhaps in shallow-water communities. Alternatively, the carbon may have originated by Fischer–Tropsch synthesis at ocean hydrothermal vents. The observed lateral continuity of BIF layers may perhaps be explained by chemical signaling by the bacteria of favorable or unfavorable environmental conditions, leading to nearly synchronous cell morphogenesis from a vegetative to resting phase and vice versa.

Earth and Planetary Science Letters↗

USGS2021

Material failure and caldera collapse: Insights from the 2018 Kilauea eruption

The Failure Forecast Method (FFM) was introduced as an empirical model for forecasting catastrophic material failures related to natural hazards, such as landslides and volcanic eruptions, with mixed success. During the 2018 eruption of Kilauea volcano, Hawaii, the draining of the summit magma reservoir into the Lower East Rift Zone resulted in the formation of a new caldera at the summit. I tested the applicability of the FFM to caldera collapse by analyzing the cyclical earthquake swarms and ground deformation that occurred between 62 sudden major caldera collapse events. The progression of both the cumulative moment release of the cyclical earthquakes and the GNSS displacement show a major change in mid-June. In late May through early June, the progression of the parameters is consistent with strain localization or creep progression related to the development or activation of the ring fault system. From late June until the end of the eruption, parameter progression is roughly steady with initial accelerating increases in cumulative moment and displacement that shift to approximately linear progression. Analysis of repeating earthquake families in the cyclical swarms showed that the behavior of the repeaters was consistent with that of the cyclical swarms as a whole and suggested that each family undergoes its own progression of activation to termination. While the FFM analysis identified the system change in mid-June, it did not demonstrate an ability to forecast collapse events or the end of the eruption.

Hawaii↗

USGS2010

Canopy gap dynamics of second-growth red spruce-northern hardwood stands in West Virginia

Forest restoration requires an understanding of the natural disturbance regime of the target community and estimates of the historic range of variability of ecosystem components (composition, structure, and disturbance processes). Management prescriptions that support specific restoration activities should be consistent with these parameters. In this study, we describe gap-phase dynamics of even-aged, second-growth red spruce-northern hardwood stands in West Virginia that have been significantly degraded following early Twentieth Century harvesting and wildfire. In the current stage of stand development, gaps tended to be small, with mean canopy gap and extended canopy gap sizes of 53.4m2 and 199.3m2, respectively, and a canopy turnover rate of 1.4%year-1. The majority of gaps resulted from the death of one or two trees. American beech snags were the most frequent gap maker, partially due to the elevated presence of beech-bark disease in the study area. Gaps ranged in age from 1 to 28 years, had a mean of 13 years, and were unimodal in distribution. We projected red spruce to be the eventual gap filler in approximately 40% of the gaps. However, we estimated that most average-sized gaps will close within 15-20 years before red spruce canopy ascension is projected (30-60 years). Accordingly, many understory red spruce will require more than one overhead release - an observation verified by the tree-ring record and consistent with red spruce life history characteristics. Based on our observations, silvicultural prescriptions that include overhead release treatments such as thinning from above or small gap creation through selection harvesting could be an appropriate activity to foster red spruce restoration in the central Appalachians. ?? 2010 Elsevier B.V.

Forest Ecology and Management↗

USGS2014

Tree growth and recruitment in a leveed floodplain forest in the Mississippi River Alluvial Valley, USA

Flooding is a defining disturbance in floodplain forests affecting seed germination, seedling establishment, and tree growth. Globally, flood control, including artificial levees, dams, and channelization has altered flood regimes in floodplains. However, a paucity of data are available in regards to the long-term effects of levees on stand establishment and tree growth in floodplain forests. In this study, we used dendrochronological techniques to reconstruct tree recruitment and tree growth over a 90-year period at three stands within a ring levee in the Mississippi River Alluvial Valley (MAV) and to evaluate whether recruitment patterns and tree growth changed following levee construction. We hypothesized that: (1) sugarberry is increasing in dominance and overcup oak ( Quercus lyrata ) is becoming less dominant since the levee, and that changes in hydrology are playing a greater role than canopy disturbance in these changes in species dominance; and (2) that overcup oak growth has declined following construction of the levee and cessation of overbank flooding whereas that of sugarberry has increased. Recruitment patterns shifted from flood-tolerant overcup oak to flood-intolerant sugarberry ( Celtis laevigata ) after levee construction. None of the 122 sugarberry trees cored in this study established prior to the levee, but it was the most common species established after the levee. The mechanisms behind the compositional change are unknown, however, the cosmopolitan distribution of overcup oak during the pre-levee period and sugarberry during the post-levee period, the lack of sugarberry establishment in the pre-levee period, and the confinement of overcup oak regeneration to the lowest areas in each stand after harvest in the post-levee period indicate that species-specific responses to flooding and light availability are forcing recruitment patterns. Overcup oak growth was also affected by levee construction, but in contrast to our hypothesis, growth actually increased for several decades before declining during a drought in the late 1990s. We interpret this result as removal of flood stress following levee construction. This finding emphasizes the fact that flooding can be stressful to trees regardless of their flood tolerance and that growth in floodplain trees can be sustained provided adequate soil moisture is present, regardless of the source of soil moisture. However, future research efforts should focus on the long-term effect of hydrologic modification on stand development and on how hydrologic modifications, such as elimination of surface flooding and groundwater declines, affect the vulnerability of floodplain forests to drought.

Forest Ecology and Management↗

USGS2019

Whitebark pine (Pinus albicaulis) growth and defense in response to mountain pine beetle outbreaks

Whitebark pine (Pinus albicaulis) is a critical forest species of Northern Rocky Mountain upper subalpine ecosystems, yet little is known about the physiological response of whitebark pine to disturbance (e.g. fire, bark beetles, and pathogens) across a range of diverse environmental gradients. Resin–based defenses have long been recognized as the primary mechanism by which conifers respond to attack by bark beetles and pathogens and several studies have linked resin duct properties to survivorship during periods of increased beetle activity. However, to our knowledge, no studies have compared axial resin ducts in the secondary xylem of whitebark pine across pairs of living and dead whitebark pine trees to better understand survivorship following multiple disturbances including mountain pine beetle and white pine blister rust. We found a clear distinction in growth and defense characteristics between live and dead whitebark pine. Across our study sites on the Flathead Indian Reservation in northwestern Montana, live whitebark pine produced larger resin ducts with a greater annual investment in resin–based defenses than whitebark pine that died. Resin duct size, duct area, and relative duct area were all greater in live whitebark pine (by 56%, 48%, and 57%, respectively) and these were the most important variables influencing whitebark pine survivorship. In contrast, whitebark pine that had died grew faster over time (22% larger ring widths) than their live counterparts and also produced more resin duct structures (20% more ducts on average). Whitebark pine at our study sites exhibit differing strategies in the allocation of resources toward growth and defense, with the majority of survivors of recent disturbance investing more in defensive structures than growth. Our results support the idea that maintaining genetic variability and the associated suite of differing physiological traits promotes diverse response strategies to a complex array of biophysical and biological stressors that might leave a species vulnerable to extinction across its range.

Northern Rocky Mountain↗

USGS2016

Novel insights from NMR spectroscopy into seasonal changes in the composition of dissolved organic matter exported to the Bering Sea by the Yukon River

Seasonal (spring freshet, summer–autumn, and winter) variability in the chemical composition of dissolved organic matter (DOM) from the Yukon River was determined using advanced one- and two-dimensional (2D) solid-state NMR spectroscopy, coupled with isotopic measurements and UV–visible spectroscopy. Analyses were performed on two major DOM fractions, the hydrophobic organic acid (HPOA) and transphilic organic acid (TPIA) fractions obtained using XAD resins. Together these two fractions comprised 64–74% of the total DOM. Carboxyl-rich alicyclic molecules (CRAM) accounted for the majority of carbon atoms in the HPOA (63–77%) and TPIA (54–78%) samples, and more so in winter and summer than in spring samples. 2D and selective NMR data revealed association of abundant nonprotonated O-alkyl and quaternary alkyl C (OC np , OC np O and C q , 13–17% of HPOA and 15–20% of TPIA) and isolated O–CH structures with CRAM, which were not recognized in previous studies. Spectral editing and 2D NMR allowed for the discrimination of carbohydrate-like O-alkyl C from non-carbohydrate O-alkyl C. Whereas two spring freshet TPIA samples contained carbohydrate clusters such as carboxylated carbohydrates (16% and 26%), TPIA samples from other seasons or HPOA samples mostly had small amounts (<8%) of sugar rings dispersed in a nonpolar alkyl environment. Though nonprotonated aromatic C represented the largest fraction of aromatic C in all HPOA/TPIA isolates, only a small fraction (&sim;5% in HPOA and 3% in TPIA) was possibly associated with dissolved black carbon. Our results imply a relatively stable portion of DOM exported by the Yukon River across different seasons, due to the predominance of CRAM and their associated nonprotonated C–O and O–C–O structures, and elevated reactivity (bio- and photo-lability) of spring DOM due to the presence of terrestrial inputs enriched in carbohydrates and aromatic structures.

Alaska, Yukon↗

USGS2010

Fluvial processes and vegetation - Glimpses of the past, the present, and perhaps the future.

"Most research before 1960 into interactions among fluvial processes, resulting landforms, and vegetation was descriptive. Since then, however, research has become more detailed and quantitative permitting numerical modeling and applications including agricultural-erosion abatement and rehabilitation of altered bottomlands. Although progress was largely observational, the empiricism increasingly yielded to objective recognition of how vegetation interacts with and influences geomorphic process. A review of advances relating fluvial processes and vegetation during the last 50 years centers on hydrologic reconstructions from tree rings, plant indicators of flow- and flood-frequency parameters, hydrologic controls on plant species, regulation of sediment movement by vegetation, vegetative controls on mass movement, and relations between plant cover and sediment movement. Extension of present studies of vegetation as a regulator of bottomland hydrologic and geomorphic processes may become markedly more sophisticated and widespread than at present. Research emphases that are likely to continue include vegetative considerations for erosion modeling, response of riparian-zone forests to disturbance such as dams and water diversion, the effect of vegetation on channel and bottomland dynamics, and rehabilitation of stream corridors. Research topics that presently are receiving attention are the effect of woody vegetation on the roughness of stream corridors and, hence, processes of flood conveyance and flood-plain sedimentation, the development of a theoretical basis for rehabilitation projects as opposed to fully empirical approaches, the effect of invasive plant species on the dynamics of bottomland vegetation, the quantification of below-surface biomass and related soil-stability factors for use in erosion prediction models, and the effect of impoundments on downstream narrowing of channels and accompanying encroachment of vegetation. Bottomland vegetation partially controls and is controlled by fluvial-geomorphic processes. The purposes of this paper are to identify and review investigations that have related vegetation to bottomland features and processes, to distinguish the present status of these investigations, and to anticipate future research into how hydrologic and fluvial-geomorphic processes of bottomlands interact with vegetation."

Geomorphology↗

USGS2015

Patterns of floodplain sediment deposition along the regulated lower Roanoke River, North Carolina: annual, decadal, centennial scales

The lower Roanoke River on the Coastal Plain of North Carolina is not embayed and maintains a floodplain that is among the largest on the mid-Atlantic Coast. This floodplain has been impacted by substantial aggradation in response to upstream colonial and post-colonial agriculture between the mid-eighteenth and mid-nineteenth centuries. Additionally, since the mid-twentieth century stream flow has been regulated by a series of high dams. We used artificial markers (clay pads), tree-ring (dendrogeomorphic) techniques, and pollen analyses to document sedimentation rates/amounts over short-, intermediate-, and long-term temporal scales, respectively. These analyses occurred along 58 transects at 378 stations throughout the lower river floodplain from near the Fall Line to the Albemarle Sound. Present sediment deposition rates ranged from 0.5 to 3.4 mm/y and 0.3 to 5.9 mm/y from clay pad and dendrogeomorphic analyses, respectively. Deposition rates systematically increased from upstream (high banks and floodplain) to downstream (low banks) reaches, except the lowest reaches. Conversely, legacy sediment deposition (A.D. 1725 to 1850) ranged from 5 to about 40 mm/y, downstream to upstream, respectively, and is apparently responsible for high banks upstream and large/wide levees along some of the middle stream reaches. Dam operations have selectively reduced levee deposition while facilitating continued backswamp deposition. A GIS-based model predicts 453,000 Mg of sediment is trapped annually on the floodplain and that little watershed-derived sediment reaches the Albemarle Sound. Nearly all sediment in transport and deposited is derived from the channel bed and banks. Legacy deposits (sources) and regulated discharges affect most aspects of present fluvial sedimentation dynamics. The lower river reflects complex relaxation conditions following both major human alterations, yet continues to provide the ecosystem service of sediment trapping.

North Carolina↗

USGS2004

Observations and temperatures of Io's Pele Patera from Cassini and Galileo spacecraft images

Pele has been the most intense high-temperature hotspot on Io to be continuously active during the Galileo monitoring from 1996–2001. A suite of characteristics suggests that Pele is an active lava lake inside a volcanic depression. In 2000–2001, Pele was observed by two spacecraft, Cassini and Galileo. The Cassini observations revealed that Pele is variable in activity over timescales of minutes, typical of active lava lakes in Hawaii and Ethiopia. These observations also revealed that the short-wavelength thermal emission from Pele decreases with rotation of Io by a factor significantly greater than the cosine of the emission angle, and that the color temperature becomes more variable and hotter at high emission angles. This behavior suggests that a significant portion of the visible thermal emission from Pele comes from lava fountains within a topographically confined lava body. High spatial resolution, nightside images from a Galileo flyby in October 2001 revealed a large, relatively cool (<800 K) region, ringed by bright hotspots, and a central region of high thermal emission, which is hypothesized to be due to fountaining and convection in the lava lake. Images taken through different filters revealed color temperatures of 1500±80 K from Cassini ISS data and 1605±220 and 1420±100 K from small portions of Galileo SSI data. Such temperatures are near the upper limit for basaltic compositions. Given the limitations of deriving lava eruption temperature in the absence of in situ measurement , it is possible that Pele has lavas with ultramafic compositions. The long-lived, vigorous activity of what is most likely an actively overturning lava lake in Pele Patera indicates that there is a strong connection to a large, stable magma source region.

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