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USGS2008

Water-quality data for pharmaceuticals and other organic wastewater contaminants in ground water and in untreated drinking water sources in the United States, 2000-01

This report presents water-quality data from two nationwide studies on the occurrence and distribution of organic wastewater contaminants. These data are part of the continuing effort of the U.S. Geological Survey Toxic Substances Hydrology Program to collect baseline information on the environmental occurrence of pharmaceuticals and other organic wastewater contaminants. In 2000, samples were collected from 47 ambient ground-water sites (not drinking-water wells) in 18 states and analyzed for 65 organic wastewater contaminants. In the summer of 2001, samples were collected from 74 sources of raw, untreated, drinking water in 25 states and Puerto Rico and analyzed for 100 organic wastewater contaminants. These sources comprise 25 ground-water and 49 surface-water sources of drinking water serving populations ranging from one family to more than 8 million people. Site selection for both studies focused on areas known or suspected to contain sources of animal and/or human wastewater. The five most frequently detected compounds in samples collected from ambient ground-water sites are N,N-diethyltoluamide (35 percent, insect repellant), bisphenol A (30 percent, plasticizer), tri(2-chloroethy) phosphate (30 percent, fire retardant), sulfamethoxazole (23 percent, veterinary and human antibiotic), and 4-octylphenol monoethoxylate (19 percent, detergent metabolite). The five most frequently detected organic wastewater contaminants in samples of untreated drinking water from surface-water sources are cholesterol (59 percent, natural sterol), metolachlor (53 percent, herbicide), cotinine (51 percent, nicotine metabolite), β-sitosterol (37 percent, natural plant sterol), and 1,7-dimethylxanthine (27 percent, caffeine metabolite). The five most frequently detected organic wastewater contaminants in samples of untreated drinking water from ground-water sources are tetrachloroethylene (24 percent, solvent), carbamazepine (20 percent, pharmaceutical), bisphenol A (20 percent, plasticizer), 1,7-dimethylxanthine (16 percent, caffeine metabolite), and tri(2-chloroethyl) phosphate (12 percent, fire retardant).

Open-File Report↗

USGS2012

Groundwater quality and simulation of sources of water to wells in the Marsh Creek valley at the U.S. Geological Survey Northern Appalachian Research Laboratory, Tioga County, Pennsylvania

This report provides a November 2010 snapshot of groundwater quality and an analysis of the sources of water to wells at the U.S. Geological Survey (USGS) Northern Appalachian Research Laboratory (NARL) near Wellsboro, Pennsylvania. The laboratory, which conducts fisheries research, currently (2011) withdraws 1,000 gallons per minute of high-quality groundwater from three wells completed in the glacial sand and gravel aquifer beneath the Marsh Creek valley; a fourth well that taps the same aquifer provides the potable supply for the facility. The study was conducted to document the source areas and quality of the water supply for this Department of Interior facility, which is surrounded by the ongoing development of natural gas from the Marcellus Shale. Groundwater samples were collected from the four wells used by the NARL and from two nearby domestic-supply wells. The domestic-supply wells withdraw groundwater from bedrock of the Catskill Formation. Samples were analyzed for major ions, nutrients, trace metals, radiochemicals, dissolved gases, and stable isotopes of oxygen and hydrogen in water and carbon in dissolved carbonate to document groundwater quality. Organic constituents (other than hydrocarbon gases) associated with hydraulic fracturing and other human activities were not analyzed as part of this assessment. Results show low concentrations of all constituents. Only radon, which ranged from 980 to 1,310 picocuries per liter, was somewhat elevated. These findings are consistent with the pristine nature of the aquifer in the Marsh Creek valley, which is the reason the laboratory was sited at this location. The sources of water and areas contributing recharge to wells were identified by the use of a previously documented MODFLOW groundwater-flow model for the following conditions: (1) withdrawals of 1,000 to 3,000 gallons per minute from the NARL wells, (2) average or dry hydrologic conditions, and (3) withdrawals of 1,000 gallons per minute from a new well 3,500 feet to the southwest that was drilled to provide water for Marcellus gas-well operations. Results of simulations indicate that during average hydrologic conditions, infiltration from Straight Run, a tributary to Marsh Creek, provides nearly all the water to the NARL wells. During dry conditions, the areas contributing recharge expand such that Asaph Run contributes about half of the water to the NARL wells when withdrawals are 1,000 or 2,000 gallons per minute. The addition of a simulated withdrawal of 1,000 gallons per minute from the nearby new well does not substantially affect the sources of water captured by the NARL wells. These results are subject to some limitations. The water-quality samples represent a snapshot of groundwater chemistry for only one hydrologic condition; the concentrations of some constituents may change temporally. In addition, samples were collected and analyzed for hydrocarbon gases, but not organic constituents associated with hydraulic fracturing; additional sampling for these constituents would provide a more complete water-quality baseline. The sources contributing water to the NARL wells and the new well were simulated by use of a simplified one-layer model of the glacial sand and gravel aquifer for steady-state conditions that in reality are never achieved. Steady-state simulations of dry hydrologic conditions show that it is possible for the NARL wells to capture water from Asaph Run; however, maps of simulated groundwater time-of-travel indicate that a dry period of unusually long duration would be required. A better analysis could be done by recalibrating the groundwater-flow model with a finite-difference grid having multiple layers, cells smaller than the 200-foot by 200-foot cells used in this study, and transient stress periods.

Pennsylvania↗

USGS2006

Using self-organizing maps to determine observation threshold limit predictions in highly variant data

A significant data quality challenge for highly variant systems surrounds the limited ability to quantify operationally reasonable limits on the data elements being collected and provide reasonable threshold predictions. In many instances, the number of influences that drive a resulting value or operational range is too large to enable physical sampling for each influencer, or is too complicated to accurately model in an explicit simulation. An alternative method to determine reasonable observation thresholds is to employ an automation algorithm that would emulate a human analyst visually inspecting data for limits. Using the visualization technique of self-organizing maps (SOM) on data having poorly understood relationships, a methodology for determining threshold limits was developed. To illustrate this approach, analysis of environmental influences that drive the abundance of a target indicator species (the pink shrimp, Farfantepenaeus duorarum) provided a real example of applicability. The relationship between salinity and temperature and abundance of F. duorarum is well documented, but the effect of changes in water quality upstream on pink shrimp abundance is not well understood. The highly variant nature surrounding catch of a specific number of organisms in the wild, and the data available from up-stream hydrology measures for salinity and temperature, made this an ideal candidate for the approach to provide a determination about the influence of changes in hydrology on populations of organisms.

Conference Paper↗

USGS2018

When oil and water mix: Understanding the environmental impacts of shale development

Development of shale gas and tight oil, or unconventional oil and gas (UOG), has dramatically increased domestic energy production in the U.S. UOG resources are typically developed through the use of hydraulic fracturing, which creates high-permeability flow paths into large volumes of tight rocks to provide a means for hydrocarbons to move to a wellbore. This process uses significant volumes of water, sand, and chemicals, raising concerns about risks to the environment and to human health. Researchers in various disciplines have been working to make UOG development more efficient, and to better understand the risks to air quality, water quality, landscapes, human health, and ecosystems. Risks to air include releases of methane, carbon dioxide, volatile organic compounds, and particulate matter. Water-resource risks include excessive withdrawals, stray gas in drinking-water aquifers, and surface spills of fluids or chemicals. Landscapes can be significantly altered by the infrastructure installed to support large drilling platforms and associated equipment. Exposure routes, fate and transport, and toxicology of chemicals used in the hydraulic fracturing process are poorly understood, as are the potential effects on terrestrial and aquatic ecosystems and human health. This is made all the more difficult by an adaptable and evolving industry that frequently changes methods and constantly introduces new chemicals. Geoscientists responding to questions about the risks of UOG should refer to recent, rigorous scientific research.

GSA Today↗

USGS2007

State factor relationships of dissolved organic carbon and nitrogen losses from unpolluted temperate forest watersheds

We sampled 100 unpolluted, old-growth forested watersheds, divided among 13 separate study areas over 5 years in temperate southern Chile and Argentina, to evaluate relationships among dominant soil-forming state factors and dissolved carbon and nitrogen concentrations in watershed streams. These watersheds provide a unique opportunity to examine broad-scale controls over carbon (C) and nitrogen (N) biogeochemistry in the absence of significant human disturbance from chronic N deposition and land use change. Variations in the ratio dissolved organic carbon (DOC) to nitrogen (DON) in watershed streams differed by underlying soil parent material, with average C:N = 29 for watersheds underlain by volcanic ash and basalt versus C:N = 73 for sedimentary and metamorphic parent materials, consistent with stronger adsorption of low C:N hydrophobic materials by amorphous clays commonly associated with volcanic ash and basalt weathering. Mean annual precipitation was related positively to variations in both DOC (range: 0.2-9.7 mg C/L) and DON (range: 0.008-0.135 mg N/L) across study areas, suggesting that variations in water volume and concentration may act synergistically to influence C and N losses across dry to wet gradients in these forest ecosystems. Dominance of vegetation by broadleaf versus coniferous trees had negligible effects on organic C and N concentrations in comparison to abiotic factors. We conclude that precipitation volume and soil parent material are important controls over chemical losses of dissolved organic C and N from unpolluted temperate forest watersheds. Our results raise the possibility that biotic imprints on watershed C and N losses may be less pronounced in naturally N-poor forests than in areas impacted by land use change and chronic N deposition. Copyright 2007 by the American Geophysical Union.

Journal of Geophysical Research G: Biogeosciences↗

USGS1994

Alternative tissue analysis method developed for organochlorine contaminants in aquatic organisms

The exposure of aquatic life to organochlorine contaminants has been investigated during the past two decades because of human and ecosystem health concerns related to the bioaccumulation of hazardous, lipophilic substances. The toxic effects of polychlorodibenzo-12-dioxins and polychlorinated biphenyls (PCBs) are well known, and recent evidence also suggests that low level exposure to lipophilic organochlorines may interfere with normal development during sensitive early life history stages (Hileman 1993). As the use of lipophilic organochlorines, such as DDT, in third world countries continues and with the purported global cycling (Bidleman and Olney 1974; Tanabe et al. 1983) and food chain accumulation (Thomann and Connoly 1984, Thomann 1989) of persistent organochlodnes, the occurrence of these compounds in aquatic organisms is a critical global environmental issue. An understanding of the fate of organochlorines in the environment clearly remains an extremely important subject related to water quality. The U.S. Geological Survey (USGS) has recently gained congressional approval in the United States to track nation wide trends in water quality through the establishment of the National Water Quality Assessment Program (NAWQA). Among the goals defined by NAWQA, aquatic organisms, including fish, shellfish, and plants, collected from major drainage basins will be analyzed for, along with other contaminants, polychlorinated biphenyls (PCBs), organochlorine insecticides, and chlorobenzenes (Crawford and Luoma 1992). The purpose of this report is to present quality assurance data obtained from the development of a PCB, chlorobenzene, and organochlorine insecticide tissue analysis method in support of NAWQA and other large-scale water quality programs conducted through our laboratory.

Bulletin of Environmental Contamination and Toxico↗

USGS2013

Occurrence and mobility of mercury in groundwater: Chapter 5

1. Introduction 1.1. FORMS, TOXICITY, AND HEALTH EFFECTS Mercury (Hg) has long been identified as an element that is injurious, even lethal, to living organisms. Exposure to its inorganic form, mainly from elemental Hg (Hg(0)) vapor ( Fitzgerald & Lamborg, 2007 ) can cause damage to respiratory, neural, and renal systems ( Hutton, 1987 ; USEPA, 2012 ; WHO, 2012 ). The organic form, methylmercury (CH 3 Hg + ; MeHg), is substantially more toxic than the inorganic form ( Fitzgerald & Lamborg, 2007 ). Methylmercury attacks the nervous system and exposure can prove lethal, as demonstrated by well-known incidents such as those in 1956 in Minimata, Japan ( Harada, 1995 ), and 1971 in rural Iraq ( Bakir et al., 1973 ), where, in the former, industrial release of MeHg into coastal waters severely tainted the fish caught and eaten by the local population, and in the latter, grain seed treated with an organic mercurial fungicide was not planted, but eaten in bread instead. Resultant deaths are not known with certainty but have been estimated at about 100 and 500, respectively ( Hutton, 1987 ). Absent such lethal accidents, human exposure to MeHg comes mainly from ingestion of piscivorous fish in which MeHg has accumulated, with potential fetal damage ascribed to high fish diets during their mothers’ pregnancies ( USEPA, 2001 ). Lesser human exposure occurs through ingestion of drinking water (USEPA, 2001), where concentrations of total Hg (THg; inorganic plus organic forms) typically are in the low nanograms-per-liter range [1] - , particularly from many groundwater sources, and concentrations at the microgram-per-liter level are rare.

Book chapter↗

USGS2016

A revision in hydrogen isotopic composition of USGS42 and USGS43 human-hair stable isotopic reference materials for forensic science

The hydrogen isotopic composition ( δ 2 H VSMOW-SLAP ) of USGS42 and USGS43 human hair stable isotopic reference materials, normalized to the VSMOW (Vienna-Standard Mean Ocean Water)–SLAP (Standard Light Antarctic Precipitation) scale, was originally determined with a high temperature conversion technique using an elemental analyzer (TC/EA) with a glassy carbon tube and glassy carbon filling and analysis by isotope-ratio mass spectrometer (IRMS). However, the TC/EA IRMS method can produce inaccurate δ 2 H VSMOW-SLAP results when analyzing nitrogen-bearing organic substances owing to the formation of hydrogen cyanide (HCN), leading to non-quantitative conversion of a sample into molecular hydrogen (H 2 ) for IRMS analysis. A single-oven, chromium-filled, elemental analyzer (Cr-EA) coupled to an IRMS substantially improves the measurement quality and reliability of hydrogen isotopic analysis of hydrogen- and nitrogen-bearing organic material because hot chromium scavenges all reactive elements except hydrogen. USGS42 and USGS43 human hair isotopic reference materials have been analyzed with the Cr-EA IRMS method, and the δ 2 H VSMOW-SLAP values of their non-exchangeable hydrogen fractions have been revised: where mUr = 0.001 = ‰. On average, these revised δ 2 H VSMOW-SLAP values are 5.7 mUr more positive than those previously measured. It is critical that readers pay attention to the δ 2 H VSMOW-SLAP of isotopic reference materials in publications as they may need to adjust the δ 2 H VSMOW–SLAP measurement results of human hair in previous publications to ensure all results are on the same isotope-delta scale.

Forensic Science International↗

USGS2011

Factors affecting groundwater quality in the Valley and Ridge aquifers, eastern United States, 1993-2002

Chemical and microbiological analyses of water from 230 wells and 35 springs in the Valley and Ridge Physiographic Province, sampled between 1993 and 2002, indicated that bedrock type (carbonate or siliciclastic rock) and land use were dominant factors influencing groundwater quality across a region extending from northwestern Georgia to New Jersey. The analyses included naturally occurring compounds (major mineral ions and radon) and anthropogenic contaminants [pesticides and volatile organic compounds (VOCs)], and contaminants, such as nitrate and bacteria, which commonly increase as a result of human activities. Natural factors, such as topographic position and the mineral composition of underlying geology, act to produce basic physical and geochemical conditions in groundwater that are reflected in physical properties, such as pH, temperature, specific conductance, and alkalinity, and in chemical concentrations of dissolved oxygen, radon, and major mineral ions. Anthropogenic contaminants were most commonly found in water from wells and springs in carbonate-rock aquifers. Nitrate concentrations exceeded U.S. Environmental Protection Agency maximum contaminant levels in 12 percent of samples, most of which were from carbonate-rock aquifers. Escherichia coli (E. coli), pesticide, and VOC detection frequencies were significantly higher in samples from sites in carbonate-rock aquifers. Naturally occurring elements, such as radon, iron, and manganese, were found in higher concentrations in siliciclastic-rock aquifers. Radon levels exceeded the proposed maximum contaminant level of 300 picocuries per liter in 74 percent of the samples, which were evenly distributed between carbonate- and siliciclastic-rock aquifers. The land use in areas surrounding wells and springs was another significant explanatory variable for the occurrence of anthropogenic compounds. Nitrate and pesticide concentrations were highest in samples collected from sites in agricultural areas and lowest in samples collected from sites in undeveloped areas. Volatile organic compounds were detected most frequently and in highest concentrations in samples from sites in urban areas, and least frequently in agricultural and undeveloped areas. No volatile organic compound concentrations and concentrations from only one pesticide, dieldrin, exceeded human-health benchmarks.

Alabama;Georgia;Tennessee;North Carolina;Virginia;↗

USGS2014

Status and understanding of groundwater quality in the Klamath Mountains study unit, 2010: California GAMA Priority Basin Project

Groundwater quality in the Klamath Mountains (KLAM) study unit was investigated as part of the Priority Basin Project of the California Groundwater Ambient Monitoring and Assessment (GAMA) Program. The study unit is located in Del Norte, Humboldt, Shasta, Siskiyou, Tehama, and Trinity Counties. The GAMA Priority Basin Project is being conducted by the California State Water Resources Control Board in collaboration with the U.S. Geological Survey (USGS) and the Lawrence Livermore National Laboratory. The GAMA Priority Basin Project was designed to provide a spatially unbiased, statistically robust assessment of the quality of untreated (raw) groundwater in the primary aquifer system. The assessment is based on water-quality data and explanatory factors for groundwater samples collected in 2010 by the USGS from 39 sites and on water-quality data from the California Department of Public Health (CDPH) water-quality database. The primary aquifer system was defined by the depth intervals of the wells listed in the CDPH water-quality database for the KLAM study unit. The quality of groundwater in the primary aquifer system may be different from that in the shallower or deeper water-bearing zones; shallow groundwater may be more vulnerable to surficial contamination. This study included two types of assessments: (1) a status assessment , which characterized the status of the current quality of the groundwater resource by using data from samples analyzed for volatile organic compounds, pesticides, and naturally occurring inorganic constituents, such as major ions and trace elements, and (2) an understanding assessment , which evaluated the natural and human factors potentially affecting the groundwater quality. The assessments were intended to characterize the quality of groundwater resources in the primary aquifer system of the KLAM study unit, not the quality of treated drinking water delivered to consumers by water purveyors. Relative-concentrations (sample concentrations divided by the health- or aesthetic-based benchmark concentrations) were used for evaluating groundwater quality for those constituents that have Federal or California regulatory or non-regulatory benchmarks for drinking-water quality. A relative-concentration greater than (>) 1.0 indicates a concentration greater than a benchmark, and a relative-concentration less than or equal to (≤) 1.0 indicates a concentration less than or equal to a benchmark. Relative-concentrations of organic constituents were classified as “high” (relative-concentration > 1.0), “moderate” (0.1 < relative-concentration ≤ 1.0), or “low” (relative-concentration ≤ 0.1). For inorganic constituents, the boundary between low and moderate relative-concentration was set at 0.5. Aquifer-scale proportion was used in the status assessment as the primary metric for evaluating regional-scale groundwater quality. High aquifer-scale proportion is defined as the percentage of the area of the primary aquifer system with a relative-concentration greater than 1.0 for a particular constituent or class of constituents; percentage is based on an areal rather than a volumetric basis. Moderate and low aquifer-scale proportions were defined as the percentages of the primary aquifer system with moderate and low relative-concentrations, respectively. The KLAM study unit includes more than 8,800 square miles (mi 2 ), but only those areas near the sampling sites, about 920 mi 2 , are included in the areal assessment of the study unit. Two statistical approaches—grid-based and spatially weighted—were used to evaluate aquifer-scale proportions for individual constituents and classes of constituents. To confirm this methodology, 90 percent confidence intervals were calculated for the grid-based high aquifer-scale proportions and were compared to the spatially weighted results, which were found to be within these confidence intervals in all cases. Grid-based results were selected for use in the status assessment unless, as was observed in a few cases, a grid-based result was zero and the spatially weighted result was not zero, in which case, the spatially weighted result was used. The status assessment showed that inorganic constituents with human-health benchmarks were detected at high relative-concentrations in 2.6 percent of the primary aquifer system and at moderate relative-concentrations in 10 percent of the system. The high aquifer-scale proportion for inorganic constituents mainly reflected the high aquifer-scale proportions of boron. Inorganic constituents with secondary maximum contaminant levels were detected at high relative-concentrations in 13 percent of the primary aquifer system and at moderate relative-concentrations in 10 percent of the system. The constituents present at high relative-concentrations included iron and manganese. Organic constituents with human-health benchmarks were not detected at high relative-concentrations, but were detected at moderate relative-concentrations in 1.9 percent of the primary aquifer system. The 1.9 percent reflected a spatially weighted moderate aquifer-scale proportion for the gasoline additive methyl tert-butyl ether. Of the 148 organic constituents analyzed, 14 constituents were detected. Only one organic constituent had a detection frequency of greater than 10 percent—the trihalomethane, chloroform. The second component of this study, the understanding assessment , identified the natural and human factors that may have affected the groundwater quality in the KLAM study unit by evaluating statistical correlations between water-quality constituents and potential explanatory factors. The potential explanatory factors evaluated were aquifer lithology, land use, hydrologic conditions, depth, groundwater age, and geochemical conditions. Results of the statistical evaluations were used to explain the occurrence and distribution of constituents in the KLAM study unit. Groundwater age distribution (modern, mixed, or pre-modern), redox class (oxic, mixed, or anoxic), and dissolved oxygen concentration were the explanatory factors that best explained occurrence patterns of the inorganic constituents. High concentrations of boron were found to be associated with groundwater classified as mixed or pre-modern with respect to groundwater age. Boron was also negatively correlated to dissolved oxygen and positively correlated to specific conductance. Iron and manganese concentrations were strongly associated with low dissolved oxygen concentrations, anoxic and mixed redox classifications, and pre-modern groundwater. Specific conductance concentrations were found to be related to pre-modern groundwater, low dissolved oxygen concentrations, and high pH. Chloroform was selected for additional evaluation in the understanding assessment because it was detected in more than 10 percent of wells sampled in the KLAM study unit. Septic tank density was the only explanatory factor that was found to relate to chloroform concentrations.

California↗

USGS2014

Use of dynamic occupancy models to assess the response of Darters (Teleostei: Percidae) to varying hydrothermal conditions in a southeastern United States tailwater

During the past 100 years, most large rivers in North America have been altered for flood control, hydropower, navigation or water supply development. Although these activities clearly provide important human services, their associated environmental disturbances can profoundly affect stream-dwelling organisms. We used dynamic multi-species occupancy models combined with a trait-based approach to estimate the influence of site-level and species-level characteristics on patch dynamic rates for 15 darter species native to the Elk River, a large, flow-regulated Tennessee River tributary in Tennessee and Alabama. Dynamic occupancy modelling results indicated that for every 2.5 °C increase in stream temperature, darters were 3.94 times more likely to colonize previously unoccupied stream reaches. Additionally, large-bodied darter species were 3.72 times more likely to colonize stream reaches compared with small-bodied species, but crevice-spawning darter species were 5.24 times less likely to colonize previously unoccupied stream reaches. In contrast, darters were 2.21 times less likely to become locally extinct for every 2.5 °C increase in stream temperature, but high stream discharge conditions elevated the risk of local extinction. Lastly, the presence of populations in neighbouring upstream study reaches contributed to a lower risk of extinction, whereas the presence of populations in neighbouring downstream study reaches contributed to higher rates of colonization. Our study demonstrates the application of a trait-based approach combined with a metapopulation framework to assess the patch dynamics of darters in a regulated river. Results from our study will provide a baseline for evaluating the ecological consequences of alternative dam operations.

River Research and Applications↗

USGS2006

Toxicogenomics in regulatory ecotoxicology

Recently, we have witnessed an explosion of different genomic approaches that, through a combination of advanced biological, instrumental, and bioinformatic techniques, can yield a previously unparalleled amount of data concerning the molecular and biochemical status of organisms. Fueled partially by large, well-publicized efforts such as the Human Genome Project, genomic research has become a rapidly growing topical area in multiple biological disciplines. Since 1999, when the term “toxicogenomics” was coined to describe the application of genomics to toxicology (1), a rapid increase in publications on the topic has occurred (Figure 1). The potential utility of toxicogenomics in toxicological research and regulatory activities has been the subject of scientific discussions and, as with any new technology, has evoked a wide range of opinion (2–6).

Environmental Science & Technology↗

USGS2022

Natural and anthropogenic landscape factors shape functional connectivity of an ecological specialist in urban Southern California

Identifying how natural (i.e., unaltered by human activity) and anthropogenic landscape variables influence contemporary functional connectivity in terrestrial organisms can elucidate the genetic consequences of environmental change. We examine population genetic structure and functional connectivity among populations of a declining species, the Blainville's horned lizard ( Phrynosoma blainvillii ), in the urbanized landscape of the Greater Los Angeles Area in Southern California, USA. Using single nucleotide polymorphism data, we assessed genetic structure among populations occurring at the interface of two abutting evolutionary lineages, and at a fine scale among habitat fragments within the heavily urbanized area. Based on the ecology of P. blainvillii , we predicted which environmental variables influence population structure and gene flow and used gravity models to distinguish among hypotheses to best explain population connectivity. Our results show evidence of admixture between two evolutionary lineages and strong population genetic structure across small habitat fragments. We also show that topography, microclimate, and soil and vegetation types are important predictors of functional connectivity, and that anthropogenic disturbance, including recent fire history and urban development, are key factors impacting contemporary population dynamics. Examining how natural and anthropogenic sources of landscape variation affect contemporary population genetics is critical to understanding how to best manage sensitive species in a rapidly changing landscape.

California↗

USGS1999

Bottom sediments of Lorence Creek Lake, San Antonio, Texas, reflect contaminant trends in an urbanizing watershed

Historical use of pesticides and rapid urbanization have left their mark on the chemistry of bottom sediments in Lorence Creek Lake (fig. 1) in the northern part of San Antonio, Tex. Several metals, organochlorine compounds (pesticides and polychlorinated biphenyls [PCBs]), and polycyclic aromatic hydrocarbons (PAHs) detected in bottom sediments of the lake have temporal trends indicating anthropogenic (human) sources. Lorence Creek Lake is not unique; the same metals and organic compounds are routinely found in lake sediments in urbanizing watersheds (Van Metre and Callender, in press).

Fact Sheet↗

USGS2009

Water-Quality and Biological Assessment of the Iowa River and Tributaries Within and Contiguous to the Meskwaki Settlement of the Sac and Fox Tribe of the Mississippi in Iowa, 2006-07

In cooperation with the Sac and Fox Tribe of the Mississippi in Iowa (Meskwaki Nation), the U.S. Geological Survey conducted a 2-year baseline assessment of the chemical and biological quality of streams within the Meskwaki Settlement in central Iowa. The Meskwaki Nation is a federally recognized tribe that wishes to establish water-quality standards to safeguard the integrity of surface waters and aquatic biota within the settlement for the health and welfare of the tribal community. The settlement is drained by the Iowa River and four tributaries (Onion, Cattail, Raven, and Bennett Creeks). Water-quality samples were collected at three sites on the Iowa River, two sites on Onion Creek, and one site each on Cattail, Raven, and Bennett Creeks from April 2006 through July 2007. Biological and habitat assessments were conducted at all three sites on the Iowa River and the downstream-most site on Onion Creek from June through August 2007. Analysis of physical properties, major ions, nutrients, trace compounds, bacteria, and total suspended solids in water, and trace metals and organic compounds in streambed sediment provided information about the effects of anthropogenic (human related) activities on the water quality of settlement streams. Analysis of biological samples collected during the summer of 2007, including fish community, benthic macroinvertebrates, and periphyton samples, as well as physical habitat characteristics, provided information on the effects of water quality on the condition of the aquatic environment. The majority of surface water sampled within the settlement was predominately a calcium bicarbonate type. Nitrates (nitrate plus nitrite as nitrogen) exceeded the U.S. Environmental Protection Agency's (USEPA) primary drinking-water Maximum Contaminant Level of 10 ug/L in 19 of 36 samples from sites on the Iowa River and Raven and Bennett Creeks but not in samples from Onion and Cattail Creeks. None of the samples analyzed for pesticides, trace metals, wastewater, or fuel contaminants were found to exceed drinking-water regulations for the USEPA or State of Iowa targeted constituents. Bacteria densities for Escherichia coli (E. coli) ranged from less than 10 to more than 600,000 colony-forming units per 100 milliliters of water and were largest following intense rainfall runoff. The largest densities were recorded in samples collected from the tributaries, most notably from Cattail Creek downstream from the tribal headquarters area and Onion Creek downstream from the sewage lagoons. Arsenic and nickel concentrations in bottom sediment from Onion Creek exceeded the USEPA threshold effects level in a composite sample collected during the habitat assessment in July 2007. Suspended-sediment concentration was estimated in terms of total suspended solids. Overall, Onion and Bennett Creeks were the least turbid, whereas the ephemeral Cattail Creek had the most turbid samples. Aquatic-community data were collected at four sites on the Meskwaki Settlement during the summer of 2007 to provide a baseline biological assessment of stream conditions. This assessment was based on sampling of the fish, benthic macroinvertebrate, and periphyton communities along with physical habitat characteristics. Individual biological metrics were derived from the data collected during the community surveys. These metrics were used to calculate Indexes of Biological Integrity (IBIs). The calculated values from the IBIs provided a numerical value that was used to provide an assessment of the biological condition at each biological sampling site. The fish community samples indicated that all of the sampling sites would be considered in fair condition, with one exception being a collection site on the Iowa River at Highway 49 near Tama, Iowa, which was classified in poor condition. The benthic macroinvertebrate IBI indicated a classification of good for three of the four biological sampling sites, with the Iowa River near Montour, Iowa,

Scientific Investigations Report↗

USGS1984

National water summary 1983: Hydrologic events and issues

The United States as a Nation possesses abundant water resources and has developed and used those resources extensively. The national renewable supply of water is about 1,400 billion gallons per day (for the conterminous 48 States). Approximately 380 billion gallons per day of freshwater is withdrawn for use by the Nation's homes, farms, and industries, and about 280 billion gallons per day is returned to streams. Although a large percentage of the Nation's waste is carried in this return flow, the quality of water in streams has improved in many respects as a result of the pollution-control pro- grams of recent years. However, much remains to be learned about water quality particularly the extent of contamination by synthetic organic chemicals and heavy metals, and the effects of these contaminants on human health.

Water Supply Paper↗

USGS1996

Summary of biological and contaminant investigations related to stream water quality and environmental setting in the Upper Colorado River basin, 1938-95

As part of the U.S. Geological Survey's National Water-Quality Assessment (NAWQA) program, an inventory of the biological and contaminant investigations for the Upper Colorado River Basin study unit was conducted. To enhance the sampling design for the biological component of the program, previous studies about the ecology of aquatic organisms and contaminants were compiled from computerized literature searches of biological data bases and by contacting other Federal, State, and local agencies. Biological and contaminant investigations that have been conducted throughout the basin since 1938 were categorized according to four general categories of biological investigations and two categories of contaminant investigations: algal communities, macroinvertebrate communities, fish communities, habitat characterization, contaminants in organism tissue, and contaminants in bed sediment. The studies were identified by their locations in two physiographic provinces, the Southern Rocky Mountains and the Colorado Plateau, and by the predominant land use in the area of the investigation. Studies on algal communities and contaminants in organism tissue and in bed sediment are limited throughout the basin. Studies on macroinvertebrate and fish communities and habitat characterization are the most abundant in the study unit. Natural and human factors can affect biological communities and their composition. Natural factors that affect background water-quality conditions are physiography, climate, geology, and soils. Algae, macroinvertebrates, and fish that are present in the Southern Rocky Mountains and the Colorado Plateau physiographic provinces vary with altitude and physical environment. Green algae and diatoms are predominant in the higher altitude streams, and blue-green, golden-brown, and green algae are predominant in the lower altitude streams. Caddisflies, mayflies, and stoneflies are the dominant macroinvertebrates in the higher altitudes, whereas aquatic worms, leeches, and dragonflies are more common at lower altitudes. Cold-water species, such as trout, are present at the higher altitudes, and warmer water species, such as catfish, carp, and suckers, are predominant at the lower altitudes. Human factors that affect water-quality conditions are mining, urbanization, agriculture, and hydrologic modifications. Mining areas can be depleted of organisms or contain a low diversity of species. Acid-tolerant algae, such as certain species of green algae and diatoms, and metal-tolerant caddisflies can be present in mining areas. Urbanized areas are located in the Southern Rocky Mountains and in the Colorado Plateau and contain species characteristic of the physiographic provinces. Agricultural areas contain species, such as blue-green algae, aquatic worms, suckers, and carp, that can tolerate organic enrichment, sedimentation, and lower concentrations of dissolved oxygen.

Water-Resources Investigations Report↗

USGS2013

Iron mineralogy and bioaccessibility of dust generated from soils as determined by reflectance spectroscopy and magnetic and chemical properties--Nellis Dunes recreational area, Nevada

Atmospheric mineral dust exerts many important effects on the Earth system, such as atmospheric temperatures, marine productivity, and melting of snow and ice. Mineral dust also can have detrimental effects on human health through respiration of very small particles and the leaching of metals in various organs. These effects can be better understood through characterization of the physical and chemical properties of dust, including certain iron oxide minerals, for their extraordinary radiative properties and possible effects on lung inflammation. Studies of dust from the Nellis Dunes recreation area near Las Vegas, Nevada, focus on characteristics of radiative properties (capacity of dust to absorb solar radiation), iron oxide mineral type and size, chemistry, and bioaccessibility of metals in fluids that simulate human gastric, lung, and phagolysosomal fluids. In samples of dust from the Nellis Dunes recreation area with median grain sizes of 2.4, 3.1, and 4.3 micrometers, the ferric oxide minerals goethite and hematite, at least some of it nanosized, were identified. In one sample, in vitro bioaccessibility experiments revealed high bioaccessibility of arsenic in all three biofluids and higher leachate concentration and bioaccessibility for copper, uranium, and vanadium in the simulated lung fluid than in the phagolysosomal fluid. The combination of methods used here to characterize mineral dust at the Nellis Dunes recreation area can be applied to global dust and broad issues of public health.

Nevada↗